1,2-Bis(4-methoxybenzyl)hydrazine

Base Information

Chemical Name:1,2-Bis(4-methoxybenzyl)hydrazine
CAS No.:81104-53-2
Molecular Formula:C16H20N2O2
Molecular Weight:272.3422
Hs Code.:
NSC Number:122502
DSSTox Substance ID:DTXSID00230901
Wikidata:Q83111654

Synonyms:1,2-Bis(4-methoxybenzyl)hydrazine;81104-53-2;NSC122502;1,2-bis[(4-methoxyphenyl)methyl]hydrazine;NSC 122502;SCHEMBL7346729;Di-(4-methoxybenzyl) hydrazine;DTXSID00230901;NYKKXRCUKXDUAL-UHFFFAOYSA-N;NSC-122502;SB81937

Suppliers and Price of 1,2-Bis(4-methoxybenzyl)hydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,2-Bis(4-methoxybenzyl)hydrazine

Chemical Property:

Vapor Pressure:2.09E-07mmHg at 25°C
Boiling Point:424.3°C at 760 mmHg
Flash Point:176.3°C
Density:1.095g/cm³
XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:272.152477885
Heavy Atom Count:20
Complexity:221

Purity/Quality:: 97% or 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)CNNCC2=CC=C(C=C2)OC

Technology Process of 1,2-Bis(4-methoxybenzyl)hydrazine

There total 2 articles about 1,2-Bis(4-methoxybenzyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81104-53-2
N,N'-bis-(4-methoxy-benzyl)-hydrazine

Guidance literature:: With sodium amalgam; ethanol;

Reference yield:

: 81104-53-2
N,N'-bis-(4-methoxy-benzyl)-hydrazine

Guidance literature:: Benzalazin 5c, H2, Pd-C;
DOI:10.1021/ja00853a034

Reference yield: 90.0%

: 22398-14-7
dimethyl (methoxymethylene)malonate

: 81104-53-2
N,N'-bis-(4-methoxy-benzyl)-hydrazine

: methyl 1,2-bis(4-methoxybenzyl)-3-oxo-2,3-dihydro-1H-pyrazole-4-carboxylate

Guidance literature:: N,N'-bis-(4-methoxy-benzyl)-hydrazine; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

dimethyl (methoxymethylene)malonate; In tetrahydrofuran; at 0 - 25 ℃; for 2.5h; Inert atmosphere;

With toluene-4-sulfonic acid; In acetonitrile; at 25 ℃; for 0.5h;
DOI:10.1021/acs.joc.6b01237