6-[[[2-hydroxy-3-[(6-oxo-1-cyclohexa-2,4-dienylidene)methylamino]propy l]amino]methylidene]cyclohexa-2,4-dien-1-one

Base Information

• Chemical Name: 6-[[[2-hydroxy-3-[(6-oxo-1-cyclohexa-2,4-dienylidene)methylamino]propy l]amino]methylidene]cyclohexa-2,4-dien-1-one
• CAS No.: 3694-33-5
• Molecular Formula: C₁₇H₁₈N₂O₃
• Molecular Weight: 298.342
• Mol file: 3694-33-5.mol

Synonyms:2-Propanol,1,3-bis(salicylideneamino)- (7CI,8CI); 1,3-Bis(salicylidenamino)propan-2-ol; 1,3-Bis(salicylideneamino)-2-propanol;Bis(salicylidene)-2-hydroxy-1,3-propanediamine;Bis(salicylideneamino)-2-propanol;N,N'-2-Hydroxypropane-1,3-bis(salicylideneimine);N,N'-Disalicylidene-2-hydroxy-1,3-propanediamine

Chemical Property of 6-[[[2-hydroxy-3-[(6-oxo-1-cyclohexa-2,4-dienylidene)methylamino]propy l]amino]methylidene]cyclohexa-2,4-dien-1-one

Chemical Property:

• Melting Point: 100 - 102 °C
• Boiling Point: 568°Cat760mmHg
• Flash Point: 297.3°C
• PSA: 85.41000
• Density: 1.374g/cm³
• LogP: 1.99670

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-[[[2-hydroxy-3-[(6-oxo-1-cyclohexa-2,4-dienylidene)methylamino]propy l]amino]methylidene]cyclohexa-2,4-dien-1-one

There total 4 articles about 6-[[[2-hydroxy-3-[(6-oxo-1-cyclohexa-2,4-dienylidene)methylamino]propy l]amino]methylidene]cyclohexa-2,4-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.6%

salicylaldehyde (90-02-8) + 1,3-Diamino-2-hydroxypropane (616-29-5) → N,N′-bis-(salicylidene)(propylene-2-ol)-1,3-diamine (133345-52-5,3694-33-5)

Guidance literature:

In ethanol; for 8h; Reflux;

DOI:10.1016/j.ica.2020.119541

Reference yield:

2-methyl-benzyl alcohol (89-95-2) + 1,3-Diamino-2-hydroxypropane (616-29-5) → N,N′-bis-(salicylidene)(propylene-2-ol)-1,3-diamine (133345-52-5,3694-33-5)

Guidance literature:

In ethanol;

DOI:10.1039/a907668i

Reference yield:

salicylaldehyde (90-02-8) + 1,3-Diamino-2-hydroxypropane (616-29-5) → N,N′-bis-(salicylidene)(propylene-2-ol)-1,3-diamine (133345-52-5,3694-33-5) + N,N'-(salicyaldimine)-1,3-diaminopropan-2-ol (42728-82-5)

Guidance literature:

In methanol; for 2h; Reflux;

DOI:10.1016/j.tet.2009.10.060

upstream raw materials:

salicylaldehyde

1,3-Diamino-2-hydroxypropane

2-methyl-benzyl alcohol

Downstream raw materials:

N,N'-bis(2-hydroxybenzyl)-2-hydroxypropane-1,3-diamine

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