4-IODO-3-METHYLBENZONITRILE

Base Information

• Chemical Name: 4-IODO-3-METHYLBENZONITRILE
• CAS No.: 42872-85-5
• Molecular Formula: C8H6IN
• Molecular Weight: 243.047
• Hs Code.: 2926909090
• Mol file: 42872-85-5.mol

Synonyms:4-IODO-3-METHYLBENZONITRILE;

Chemical Property of 4-IODO-3-METHYLBENZONITRILE

Chemical Property:

• Vapor Pressure: 0.0015mmHg at 25°C
• Melting Point: 73-75 °C(Solv: ethanol (64-17-5))
• Boiling Point: 295.7oC at 760 mmHg
• Flash Point: 132.6oC
• PSA: 23.79000
• Density: 1.78g/cm3
• LogP: 2.47128
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

4-Iodo-3-methylbenzonitrile 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-IODO-3-METHYLBENZONITRILE

There total 2 articles about 4-IODO-3-METHYLBENZONITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

4-bromo-3-methylbenzonirtile (41963-20-6) → 4-iodo-3-methylbenzonitrile (42872-85-5)

Guidance literature:

4-bromo-3-methylbenzonirtile; With n-butyllithium; In tetrahydrofuran; methyl cyclohexane; at -65 ℃; for 2h; Inert atmosphere;

With iodine; In tetrahydrofuran; methyl cyclohexane; at -65 - 20 ℃;

DOI:10.1016/j.tetlet.2009.02.011

Reference yield:

4-amino-3-methylbenzonitrile (78881-21-7) → 4-iodo-3-methylbenzonitrile (42872-85-5)

Guidance literature:

Multistep reaction; (i) NaNO₂, aq. H₂SO₄, (ii) KI;

Reference yield: 95.0%

4-iodo-3-methylbenzonitrile (42872-85-5) → N'-hydroxy-4-iodo-3-methylbenzimidamide (1236189-44-8)

Guidance literature:

With hydroxylamine hydrochloride; sodium hydrogencarbonate; In methanol; at 20 ℃; for 2.08333h; Reflux; Inert atmosphere;

upstream raw materials:

4-amino-3-methylbenzonitrile

4-bromo-3-methylbenzonirtile

Downstream raw materials:

1-(4-iodo-3-methyl-phenyl)-ethanone

4-iodo-3-methyl-benzoyl chloride

2,4,6-tris(4-iodo-3-methylphenylene)-1,3,5-triazine

4-iodo-3-methylbenzaldehyde

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 42872-85-5 4-IODO-3-METHYLBENZONITRILE

Send

Send

Metric Ton KG G Pound L ML

Send

Send