FMOC-METYR(BZL)-OH

Base Information

Chemical Name:FMOC-METYR(BZL)-OH
CAS No.:428868-52-4
Molecular Formula:C32H29NO5
Molecular Weight:507.586
Hs Code.:2922509090
Mol file:428868-52-4.mol

Synonyms:N-(carbonyl-9H-fluoren-9-ylmethoxy)-N-methyl-L-tyrosine-O-benzyl ether;3-ethyl-1-methoxycarbonyl-1,2,5,6-tetrahydropyridine;methyl 5-ethyl-3,6-dihydro-1(2H)-pyridinecarboxylate;3-ethyl-1,2,5,6-tetrahydro-pyridine-1-carboxylic acid methyl ester;N-(carbomethoxy)-3-ethyl-1,2,5,6-tetrahydropyridine;1(2H)-Pyridinecarboxylic acid,3-ethyl-5,6-dihydro-,methyl ester;N-(9H-fluoren-9-ylmethoxycarbonyl)-N-methyl-L-tyrosine-O-benzyl ether;1-carbomethoxy-3-ethyl-1,2,5,6-tetrahydropyridine;

Suppliers and Price of FMOC-METYR(BZL)-OH

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
Fmoc-N-methyl-O-benzyl-L-tyrosine
250mg
$ 347.00

TRC
Fmoc-nα-methyl-o-benzyl-l-tyrosine
50mg
$ 75.00

Matrix Scientific
Fmoc-Nalpha-methyl-O-benzyl-L-tyrosine
1g
$ 284.00

Matrix Scientific
Fmoc-Nalpha-methyl-O-benzyl-L-tyrosine
5g
$ 1043.00

Crysdot
(S)-2-((((9H-Fluoren-9-yl)methoxy)carbonyl)(methyl)amino)-3-(4-(benzyloxy)phenyl)propanoicacid 95+%
5g
$ 623.00

ChemPep
Fmoc-N-Me-Tyr(Bzl)-OH
25g
$ 1920.00

ChemPep
Fmoc-N-Me-Tyr(Bzl)-OH
5g
$ 640.00

Chem-Impex
Fmoc--methyl--benzyl-L-tyrosine ≥ 98% (HPLC)
5G
$ 662.00

Chem-Impex
Fmoc--methyl--benzyl-L-tyrosine ≥ 98% (HPLC)
1G
$ 150.00

Chem-Impex
Fmoc-N-methyl-O-benzyl-L-tyrosine,98%(HPLC) 98%(HPLC)
250MG
$ 81.20

Total 11 raw suppliers

Chemical Property of FMOC-METYR(BZL)-OH

Chemical Property:

Boiling Point:698.3±55.0 °C(Predicted)
PKA:2.97±0.10(Predicted)
PSA：76.07000
Density:1.259±0.06 g/cm3(Predicted)
LogP:6.14220
Storage Temp.:Store at 0-5°C

Purity/Quality:

99.0% ^*data from raw suppliers

Fmoc-N-methyl-O-benzyl-L-tyrosine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses Fmoc-nalpha-methyl-o-benzyl-l-tyrosine

Technology Process of FMOC-METYR(BZL)-OH

There total 2 articles about FMOC-METYR(BZL)-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 519156-39-9
(S)-3-(9H-fluoren-9-ylmethoxycarbonyl)-4-(4-benzyloxybenzyl)oxazolidin-5-one

: 428868-52-4,1354485-25-8
N-(9H-fluoren-9-ylmethoxycarbonyl)-N-methyl-L-tyrosine-O-benzyl ether

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jo026722l

Reference yield:

: 71989-40-7
Fmoc-Tyr(Bzl)-OH

: 428868-52-4,1354485-25-8
N-(9H-fluoren-9-ylmethoxycarbonyl)-N-methyl-L-tyrosine-O-benzyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / camphorsulfonic acid / toluene / 4 h / Heating

2: 70 percent / Et₃SiH; trifluoroacetic acid / CH₂Cl₂ / 2 h / 20 °C

With triethylsilane; camphor-10-sulfonic acid; trifluoroacetic acid; In dichloromethane; toluene;
DOI:10.1021/jo026722l

Reference yield:

: C₇H₁₀NO₄Pol

: 428868-52-4,1354485-25-8
N-(9H-fluoren-9-ylmethoxycarbonyl)-N-methyl-L-tyrosine-O-benzyl ether

: C₃₉H₃₇N₂O₈Pol

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; for 1h; solid phase reaction;
DOI:10.1039/b815077j