Benzamide, 4-fluoro-N-1-naphthalenyl-

Base Information

Chemical Name:Benzamide, 4-fluoro-N-1-naphthalenyl-
CAS No.:442-72-8
Molecular Formula:C17H12FNO
Molecular Weight:265.28200
Hs Code.:

Synonyms:4-Fluoro-N-naphthalen-1-yl-benzamide;4-fluoro-benzoic acid-[1]naphthylamide;4-Fluor-benzoesaeure-[1]naphthylamid;

Suppliers and Price of Benzamide, 4-fluoro-N-1-naphthalenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-Fluoro-N-(naphthalen-1-yl)benzamide 97%
5g
$ 874.00

Chemenu
4-Fluoro-N-(naphthalen-1-yl)benzamide 97%
5g
$ 825.00

Total 5 raw suppliers

Chemical Property of Benzamide, 4-fluoro-N-1-naphthalenyl-

Chemical Property:

Melting Point:166 - 168 °C
PSA：29.10000
LogP:4.30420

Purity/Quality:

99% ^*data from raw suppliers

4-Fluoro-N-(naphthalen-1-yl)benzamide 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzamide, 4-fluoro-N-1-naphthalenyl-

There total 7 articles about Benzamide, 4-fluoro-N-1-naphthalenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 824-75-9
p-fluorobenzamide

: 90-13-1
1-Chloronaphthalene

: 442-72-8
4-fluoro-N-(naphthalen-1-yl)benzamide

Guidance literature:: With caesium carbonate; at 100 ℃; for 20h; Glovebox;
DOI:10.1021/acs.orglett.7b02024

Reference yield: 43.0%

: 90-14-2
1-Iodonaphthalene

: 140-75-0
para-fluorobenzylamine

: 442-72-8
4-fluoro-N-(naphthalen-1-yl)benzamide

Guidance literature:: With 1,10-Phenanthroline; oxygen; copper(II) bis(trifluoromethanesulfonate); potassium carbonate; In dimethyl sulfoxide; at 140 ℃; for 72h; Schlenk technique;
DOI:10.1002/adsc.201200424 DOI:10.1002/adsc.201200424

Reference yield:

: 879-18-5
naphthalene-1-carbonic acid chloride

: 442-72-8
4-fluoro-N-(naphthalen-1-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: bis(tri-ortho-tolylphosphine)palladium(0); dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine / toluene / 20 h / 130 °C / Inert atmosphere; Glovebox

2: caesium carbonate / 20 h / 100 °C / Glovebox

With bis(tri-ortho-tolylphosphine)palladium⁽⁰⁾; dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; caesium carbonate; In toluene;
DOI:10.1021/acs.orglett.7b02024