3,3''-Dimethyl-1,1':4',1''-terphenyl

Base Information

Chemical Name:3,3''-Dimethyl-1,1':4',1''-terphenyl
CAS No.:4499-84-7
Molecular Formula:C₂₀H₁₈
Molecular Weight:258.363
Hs Code.:
DSSTox Substance ID:DTXSID101291374
Nikkaji Number:J937.919C

Synonyms:DTXSID101291374;AKOS015842042;3,3''-Dimethyl-1,1':4',1''-terphenyl;J-511097

Suppliers and Price of 3,3''-Dimethyl-1,1':4',1''-terphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3,3''-Dimethyl-1,1':4',1''-terphenyl

Chemical Property:

XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:258.140850574
Heavy Atom Count:20
Complexity:256

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)C2=CC=C(C=C2)C3=CC=CC(=C3)C

Technology Process of 3,3''-Dimethyl-1,1':4',1''-terphenyl

There total 11 articles about 3,3''-Dimethyl-1,1':4',1''-terphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 106-37-6
1.4-dibromobenzene

: 17933-03-8
m-tolylboronic acid

: 4499-84-7
3,3'',-dimethyl-1,1':4',1'',-terphenyl

Guidance literature:: With potassium phosphate monohydrate; palladium dichloride; 3-(diphenylphosphino)propionic acid; In dimethyl sulfoxide; at 100 ℃; for 12h; Schlenk technique;
DOI:10.1080/00397911.2015.1126606

Reference yield: 86.0%

: 599-89-3
4-chlorophenyl p-toluenesulfonate

: 17933-03-8
m-tolylboronic acid

: 4499-84-7
3,3'',-dimethyl-1,1':4',1'',-terphenyl

Guidance literature:: With morpholine; potassium phosphate tribasic trihydrate; NHC-Pd(II)-Im; at 130 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo301270t