Carbamic acid, [1-[2,3,6,7-tetrahydro-3-methyl-7-(3-methyl-2-butenyl)-2,6-dioxo-1-(2-ox o-2-phenylethyl)-1H-purin-8-yl]-3-piperidinyl]-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: Carbamic acid, [1-[2,3,6,7-tetrahydro-3-methyl-7-(3-methyl-2-butenyl)-2,6-dioxo-1-(2-ox o-2-phenylethyl)-1H-purin-8-yl]-3-piperidinyl]-, 1,1-dimethylethyl ester
• CAS No.: 454710-78-2
• Molecular Formula: C29H38N6O5
• Molecular Weight: 550.658

Synonyms:

Chemical Property of Carbamic acid, [1-[2,3,6,7-tetrahydro-3-methyl-7-(3-methyl-2-butenyl)-2,6-dioxo-1-(2-ox o-2-phenylethyl)-1H-purin-8-yl]-3-piperidinyl]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Carbamic acid, [1-[2,3,6,7-tetrahydro-3-methyl-7-(3-methyl-2-butenyl)-2,6-dioxo-1-(2-ox o-2-phenylethyl)-1H-purin-8-yl]-3-piperidinyl]-, 1,1-dimethylethyl ester

There total 2 articles about Carbamic acid, [1-[2,3,6,7-tetrahydro-3-methyl-7-(3-methyl-2-butenyl)-2,6-dioxo-1-(2-ox o-2-phenylethyl)-1H-purin-8-yl]-3-piperidinyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

8-bromo-3-methyl-7-(3-methyl-but-2-enyl)-1-(2-oxo-2-phenyl-ethyl)-3,7-dihydro-purine-2,6-dione (875877-40-0) + t-butyl piperidin-3-ylcarbamate (184637-48-7,172603-05-3) → 1-(2-phenyl-2-oxo-ethyl)-3-methyl-7-(3-methyl-2-buten-1-yl)-8-[3-(tert.-butyloxycarbonylamino)-piperidin-1-yl]-xanthine (454710-78-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 75 ℃; for 6h;

DOI:10.1021/jm701280z

Reference yield:

→ 1-(2-phenyl-2-oxo-ethyl)-3-methyl-7-(3-methyl-2-buten-1-yl)-8-[3-(tert.-butyloxycarbonylamino)-piperidin-1-yl]-xanthine (454710-78-2)

Guidance literature:

Reference yield:

1-(2-phenyl-2-oxo-ethyl)-3-methyl-7-(3-methyl-2-buten-1-yl)-8-[3-(tert.-butyloxycarbonylamino)-piperidin-1-yl]-xanthine (454710-78-2) → 1-(2-hydroxy-2-phenyl-ethyl)-3-methyl-7-(3-methyl-2-buten-1-yl)-8-[3-(tert.-butyloxycarbonylamino)-piperidin-1-yl]-xanthine (454712-68-6)

Guidance literature:

With sodium borohydrid; In methanol;

upstream raw materials:

8-bromo-3-methyl-7-(3-methyl-but-2-enyl)-1-(2-oxo-2-phenyl-ethyl)-3,7-dihydro-purine-2,6-dione

t-butyl piperidin-3-ylcarbamate

Downstream raw materials:

1-(2-hydroxy-2-phenyl-ethyl)-3-methyl-7-(3-methyl-2-buten-1-yl)-8-[3-(tert.-butyloxycarbonylamino)-piperidin-1-yl]-xanthine

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