N-(11-Bromoundecyl)carbamic acid tert-butyl ester

Base Information

Chemical Name:N-(11-Bromoundecyl)carbamic acid tert-butyl ester
CAS No.:463930-53-2
Molecular Formula:C16H32BrNO2
Molecular Weight:350.33500
Hs Code.:
Mol file:463930-53-2.mol

Synonyms:tert-butyl 11-bromo-undecanoate;N-tert-butoxycarbonyl-11-bromoundecyl-1-amine;11-bromoundecanoic acid tert-butyl ester;Undecanoic acid,11-bromo-,1,1-dimethylethyl ester;t-butyl 11-bromoundecanoate;tert-butyl 11-bromoundecylcarbamate;

Suppliers and Price of N-(11-Bromoundecyl)carbamic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl(11-bromoundecyl)carbamate 97%
5g
$ 1836.00

Crysdot
tert-Butyl(11-bromoundecyl)carbamate 97%
1g
$ 611.00

Acrotein
11-(Boc-amino)-1-undecylbromide 97%
0.5g
$ 458.34

ACHEMBLOCK
11-(Boc-amino)-1-undecylbromide 95%
1G
$ 865.00

ACHEMBLOCK
11-(Boc-amino)-1-undecylbromide 95%
250MG
$ 340.00

ACHEMBLOCK
11-(Boc-amino)-1-undecylbromide 95%
100MG
$ 205.00

Total 6 raw suppliers

Chemical Property of N-(11-Bromoundecyl)carbamic acid tert-butyl ester

Chemical Property:

Melting Point:60-62℃
PSA：41.82000
Density:1.101
LogP:5.62130

Purity/Quality:

98% ,99% , ^*data from raw suppliers

tert-Butyl(11-bromoundecyl)carbamate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(11-Bromoundecyl)carbamic acid tert-butyl ester

There total 6 articles about N-(11-Bromoundecyl)carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 4772-51-4
11-bromoundecan-1-amine hydrobromide

: 463930-53-2
tert-butyl N-(11-bromoundecyl)carbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; water; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1055/s-0029-1218654

Reference yield: 74.0%

: 144191-92-4
(11-hydroxyundecyl)carbamic acid tert-butyl ester

: 463930-53-2
tert-butyl N-(11-bromoundecyl)carbamate

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In benzene; at 23 ℃; for 12h;
DOI:10.1021/ja0500714

Reference yield:

: 27780-89-8
11-aminoundecan-1-ol

: 463930-53-2
tert-butyl N-(11-bromoundecyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / Et₃N / CH₂Cl₂ / 10 h / 0 - 23 °C

2: 74 percent / N-bromosuccinimide; Ph₃P / benzene / 12 h / 23 °C

With N-Bromosuccinimide; triethylamine; triphenylphosphine; In dichloromethane; benzene;
DOI:10.1021/ja0500714