4,4'-dimethoxy-2,2',5,5'-tetramethyl-1,1'-biphenyl

Base Information

Chemical Name:4,4'-dimethoxy-2,2',5,5'-tetramethyl-1,1'-biphenyl
CAS No.:47052-31-3
Molecular Formula:C18H22O2
Molecular Weight:270.36600
Hs Code.:
Mol file:47052-31-3.mol

Synonyms:2,2'-5,5'-Tetramethyl-4,4'-dimethoxybiphenyl;4,4'-Dimethoxy-2,5,2',5'-tetramethyl-biphenyl;4,4'-dimethoxy-2,2',5,5'-tetramethylbiphenyl;

Suppliers and Price of 4,4'-dimethoxy-2,2',5,5'-tetramethyl-1,1'-biphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-dimethoxy-2,2',5,5'-tetramethyl-1,1'-biphenyl

Chemical Property:

Melting Point:114 - 116 °C (petroleum ether)
PSA：18.46000
LogP:4.60440

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,4'-dimethoxy-2,2',5,5'-tetramethyl-1,1'-biphenyl

There total 3 articles about 4,4'-dimethoxy-2,2',5,5'-tetramethyl-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1706-11-2
2,5-Dimethyl-anisol

: 47052-31-3
2,2',5,5'-tetramethyl-4,4'-dimethoxybiphenyl

Guidance literature:: With molybdenum(V) chloride; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1055/s-2004-830870

Reference yield:

: 95-87-4
2,5-Dimethylphenol

: 47052-31-3
2,2',5,5'-tetramethyl-4,4'-dimethoxybiphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 18 h / 65 °C

2: tert-butylammonium hexafluorophosphate(V) / Electrolysis; Green chemistry

With tert-butylammonium hexafluorophosphate(V); potassium carbonate; In acetone;
DOI:10.1002/anie.201712718