(3beta,5alpha)-4-Methylstigmasta-7,24(28)-dien-3-ol

Base Information

Chemical Name:(3beta,5alpha)-4-Methylstigmasta-7,24(28)-dien-3-ol
CAS No.:11040-28-1
Molecular Formula:C30H50 O
Molecular Weight:426.726
Hs Code.:
European Community (EC) Number:234-269-2
Nikkaji Number:J227.033A
Mol file:11040-28-1.mol

Synonyms:11040-28-1;(3beta,5alpha)-4-Methylstigmasta-7,24(28)-dien-3-ol;EINECS 234-269-2;(3S,5S,9R,10S,13R,14R,17R)-4,10,13-trimethyl-17-[(Z,2R)-5-propan-2-ylhept-5-en-2-yl]-2,3,4,5,6,9,11,12,14,15,16,17-dodecahydro-1H-cyclopenta[a]phenanthren-3-ol;LPZCCMIISIBREI-GUPKAATASA-N;4-Methyl-5alpha-stigmasta-7,24(28)-diene-3beta-ol

Suppliers and Price of (3beta,5alpha)-4-Methylstigmasta-7,24(28)-dien-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of (3beta,5alpha)-4-Methylstigmasta-7,24(28)-dien-3-ol

Chemical Property:

Boiling Point:510.8°Cat760mmHg
Flash Point:224.6°C
PSA：20.23000
Density:0.98g/cm³
LogP:8.19090
XLogP3:9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:426.386166214
Heavy Atom Count:31
Complexity:716

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC=C(CCC(C)C1CCC2C1(CCC3C2=CCC4C3(CCC(C4C)O)C)C)C(C)C
Isomeric SMILES:C/C=C(/CC[C@@H](C)[C@H]1CC[C@@H]2[C@@]1(CC[C@H]3C2=CC[C@@H]4[C@@]3(CC[C@@H](C4C)O)C)C)\C(C)C

Technology Process of (3beta,5alpha)-4-Methylstigmasta-7,24(28)-dien-3-ol

There total 7 articles about (3beta,5alpha)-4-Methylstigmasta-7,24(28)-dien-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19753-67-4
3-methyl-1-(triphenylphosphoranyliden)-2-butanone

: 11040-28-1
[24(24¹)Z]-4α-methylstigmasta-7,24(24¹)-dien-3β-ol

Guidance literature:: Multi-step reaction with 4 steps

1: PhCO₂H / toluene / Heating

2: H₂ / Pd-BaSO₄ / ethyl acetate

3: (i) nBuLi, THF, hexane, (ii) (acetylation)

4: aq. K₂CO₃ / methanol

With hydrogen; potassium carbonate; benzoic acid; palladium on barium sulfate; In methanol; ethyl acetate; toluene;

Reference yield:

: (22E,24R)-4α-methyl-5α-ergosta-7,22-dien-3β-ol aceate

: 11040-28-1
[24(24¹)Z]-4α-methylstigmasta-7,24(24¹)-dien-3β-ol

Guidance literature:: Multi-step reaction with 5 steps

1: O₃, Py / CH₂Cl₂

2: PhCO₂H / toluene / Heating

3: H₂ / Pd-BaSO₄ / ethyl acetate

4: (i) nBuLi, THF, hexane, (ii) (acetylation)

5: aq. K₂CO₃ / methanol

With pyridine; hydrogen; potassium carbonate; ozone; benzoic acid; palladium on barium sulfate; In methanol; dichloromethane; ethyl acetate; toluene;

Reference yield:

: 63109-20-6
Acetic acid (3S,4S,5S,9R,10S,13R,14R,17R)-4,10,13-trimethyl-17-((S)-1-methyl-2-oxo-ethyl)-2,3,4,5,6,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

: 11040-28-1
[24(24¹)Z]-4α-methylstigmasta-7,24(24¹)-dien-3β-ol

Guidance literature:: Multi-step reaction with 4 steps

1: PhCO₂H / toluene / Heating

2: H₂ / Pd-BaSO₄ / ethyl acetate

3: (i) nBuLi, THF, hexane, (ii) (acetylation)

4: aq. K₂CO₃ / methanol

With hydrogen; potassium carbonate; benzoic acid; palladium on barium sulfate; In methanol; ethyl acetate; toluene;