3-(N,N-DIMETHYLAMINO)-2-(4-METHYLPHENYL)ACRYLALDEHYDE

Base Information

• Chemical Name: 3-(N,N-DIMETHYLAMINO)-2-(4-METHYLPHENYL)ACRYLALDEHYDE
• CAS No.: 53868-38-5
• Molecular Formula: C₁₂H₁₅NO
• Molecular Weight: 189.257
• Hs Code.: 2922399090
• Mol file: 53868-38-5.mol

Synonyms:3-(N,N-DIMETHYLAMINO)-2-(4-METHYLPHENYL)ACRYLALDEHYDE;3-(DIMETHYLAMINO)-2-(4-METHYLPHENYL)ACRYLALDEHYDE

Chemical Property of 3-(N,N-DIMETHYLAMINO)-2-(4-METHYLPHENYL)ACRYLALDEHYDE

Chemical Property:

• Vapor Pressure: 7.83E-07mmHg at 25°C
• Melting Point: 133-135°
• Boiling Point: 406.9°Cat760mmHg
• Flash Point: 173.5°C
• PSA: 20.31000
• Density: 1.008g/cm³
• LogP: 2.09640

Purity/Quality:

98%min ^*data from raw suppliers

3-(Dimethylamino)-2-(4-methylphenyl)acrylaldehyde >95% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(N,N-DIMETHYLAMINO)-2-(4-METHYLPHENYL)ACRYLALDEHYDE

There total 1 articles about 3-(N,N-DIMETHYLAMINO)-2-(4-METHYLPHENYL)ACRYLALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1.1-Dimethoxy-3-p-tolyl-propan (19191-66-3) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 2-p-tolyl-3-dimethylaminoacrolein (53868-38-5)

Guidance literature:

With COCl₂;

DOI:10.1021/jm00310a016

Reference yield: 68.0%

vanadyl acetate + 2-p-tolyl-3-dimethylaminoacrolein (53868-38-5) + 4,5-dimethyl-1,2-phenylenediamine (3171-45-7) → VO(C36H34N4) (155022-43-8)

Guidance literature:

In N,N-dimethyl-formamide; a mixt. of vanadyl acetate, diamino compound and DMF was refluxed for 0.5 h; addn. of 2-p-tolyl-3-dimethylaminoacrolein; refluxed for 6 h; N2 atm.;; cooling with ice; pptn.;;

DOI:10.1016/0020-1693(93)03734-R

Reference yield: 51.0%

vanadyl acetate + 2-p-tolyl-3-dimethylaminoacrolein (53868-38-5) + 1,2-diamino-benzene (95-54-5) → VO(C32H26N4) (155022-42-7)

Guidance literature:

In N,N-dimethyl-formamide; a mixt. of vanadyl acetate, diamino compound and DMF was refluxed for 0.5 h; addn. of 2-p-tolyl-3-dimethylaminoacrolein; refluxed for 6 h; N2 atm.;; cooling with ice; pptn.;;

DOI:10.1016/0020-1693(93)03734-R

upstream raw materials:

1.1-Dimethoxy-3-p-tolyl-propan

N,N-dimethyl-formamide

Downstream raw materials:

(6Z,8E,15Z,17E)-7,16-Di-p-tolyl-5,14-dihydro-5,9,14,18-tetraaza-dibenzo[a,h]cyclotetradecene

VO(C₃₆H₃₄N₄)

VO(C₃₂H₂₆N₄)

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