3-Hexene, 2,2,5,5-tetramethyl-3,4-bis(1,1-dimethylethyl)-

Base Information

Chemical Name:3-Hexene, 2,2,5,5-tetramethyl-3,4-bis(1,1-dimethylethyl)-
CAS No.:28923-90-2
Molecular Formula:C14H28
Molecular Weight:196.376
Hs Code.:
DSSTox Substance ID:DTXSID00183125
Nikkaji Number:J810.126D
Mol file:28923-90-2.mol

Synonyms:3-Hexene, 2,2,5,5-tetramethyl-3,4-bis(1,1-dimethylethyl)-;28923-90-2;((CH3)3C)2C=CHC(CH3)3;DTXSID00183125

Suppliers and Price of 3-Hexene, 2,2,5,5-tetramethyl-3,4-bis(1,1-dimethylethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 3-Hexene, 2,2,5,5-tetramethyl-3,4-bis(1,1-dimethylethyl)-

Chemical Property:

Vapor Pressure:0.133mmHg at 25°C
Boiling Point:224.9°Cat760mmHg
Flash Point:62.9°C
PSA：0.00000
Density:0.775g/cm³
LogP:5.05110
XLogP3:6.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:196.219100893
Heavy Atom Count:14
Complexity:194

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C=C(C(C)(C)C)C(C)(C)C

Technology Process of 3-Hexene, 2,2,5,5-tetramethyl-3,4-bis(1,1-dimethylethyl)-

There total 3 articles about 3-Hexene, 2,2,5,5-tetramethyl-3,4-bis(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 187151-15-1
3-(1,1-dimethylethyl)-2,2,5,5-tetramethylhexane-3,4-diol

: 815-24-7
Di-t-butyl ketone

: 28923-90-2
3-(1,1-dimethylethyl)-2,2,5,5-tetramethyl-3-hexene

Guidance literature:: With lithium aluminium tetrahydride; titanium(III) chloride; In tetrahydrofuran; at 75 ℃; for 6h; Irradiation;
DOI:10.1002/jlac.199719970128

Reference yield: 22.0%

: 187151-15-1
3-(1,1-dimethylethyl)-2,2,5,5-tetramethylhexane-3,4-diol

: 815-24-7
Di-t-butyl ketone

: 75-84-3
2,2-dimethyl-propanol-1

: 28923-90-2
3-(1,1-dimethylethyl)-2,2,5,5-tetramethyl-3-hexene

Guidance literature:: With lithium aluminium tetrahydride; titanium(III) chloride; at 80 ℃; for 96h;
DOI:10.1002/jlac.199719970128

Reference yield:

: 7412-67-1
neopentyl lithium

: 28923-90-2
3-(1,1-dimethylethyl)-2,2,5,5-tetramethyl-3-hexene

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Et₂O, (ii) /BRN= 473192/

2: aq. NaOH / dioxane

With sodium hydroxide; In 1,4-dioxane;
DOI:10.1021/ja01018a039