4-Pyrimidinecarboxaldehyde, oxime (7CI,8CI,9CI)

Base Information

• Chemical Name: 4-Pyrimidinecarboxaldehyde, oxime (7CI,8CI,9CI)
• CAS No.: 1073-65-0
• Molecular Formula: C₅H₅N₃O
• Molecular Weight: 123.114
• Mol file: 1073-65-0.mol

Synonyms:NSC 245210

Chemical Property of 4-Pyrimidinecarboxaldehyde, oxime (7CI,8CI,9CI)

Chemical Property:

• Vapor Pressure: 1.23mmHg at 25°C
• Melting Point: 153-154℃
• Boiling Point: 174°Cat760mmHg
• Flash Point: 59.1°C
• PSA: 58.37000
• Density: 1.28g/cm³
• LogP: 0.28470
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Pyrimidine-4-carbaldehydeOxime ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Pyrimidinecarboxaldehyde, oxime (7CI,8CI,9CI)

There total 2 articles about 4-Pyrimidinecarboxaldehyde, oxime (7CI,8CI,9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Methylpyrimidine (3438-46-8) → Pyrimidin-aldehyd-(4)-oxim (1073-65-0)

Guidance literature:

With hydrogenchloride; ethyl nitrite; In ethanol; at 0 - 20 ℃; for 2.75h;

Reference yield:

→ Pyrimidin-aldehyd-(4)-oxim (1073-65-0)

Guidance literature:

4-Methyl-pyrimidin 1. NaH in Mineraloel 2. Amylnitrit;

Reference yield: 40.0%

Pyrimidin-aldehyd-(4)-oxim (1073-65-0) → Pyrimidine-4-carbonitrile (42839-04-3)

Guidance literature:

With trichlorophosphate; In chloroform;

DOI:10.1007/BF00506042

upstream raw materials:

4-Methylpyrimidine

Downstream raw materials:

Pyrimidine-4-carbonitrile

4-acetyl pyrimidine

C-pyrimidin-4-yl-methylamine dihydrogen chloride