1-Pyrrolidinecarboxylic acid, 2-[[[(1S)-1-[(3R,4S)-1-(2-methoxy-2-oxoethyl)-2-oxo-4-phenyl-3-azetidin yl]-3-methylbutyl]amino]carbonyl]-, 2-[(4-nitrophenyl)sulfonyl]ethyl ester, (2S)-

Base Information

Chemical Name:1-Pyrrolidinecarboxylic acid, 2-[[[(1S)-1-[(3R,4S)-1-(2-methoxy-2-oxoethyl)-2-oxo-4-phenyl-3-azetidin yl]-3-methylbutyl]amino]carbonyl]-, 2-[(4-nitrophenyl)sulfonyl]ethyl ester, (2S)-
CAS No.:482598-88-9
Molecular Formula:C31H38N4O10S
Molecular Weight:658.73
Hs Code.:

1-Pyrrolidinecarboxylic acid,
2-[[[(1S)-1-[(3R,4S)-1-(2-methoxy-2-oxoethyl)-2-oxo-4-phenyl-3-azetidin
yl]-3-methylbutyl]amino]carbonyl]-, 2-[(4-nitrophenyl)sulfonyl]ethyl ester,
(2S)-

Synonyms:

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Chemical Property of 1-Pyrrolidinecarboxylic acid, 2-[[[(1S)-1-[(3R,4S)-1-(2-methoxy-2-oxoethyl)-2-oxo-4-phenyl-3-azetidin yl]-3-methylbutyl]amino]carbonyl]-, 2-[(4-nitrophenyl)sulfonyl]ethyl ester, (2S)-

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Technology Process of 1-Pyrrolidinecarboxylic acid, 2-[[[(1S)-1-[(3R,4S)-1-(2-methoxy-2-oxoethyl)-2-oxo-4-phenyl-3-azetidin yl]-3-methylbutyl]amino]carbonyl]-, 2-[(4-nitrophenyl)sulfonyl]ethyl ester, (2S)-

There total 4 articles about 1-Pyrrolidinecarboxylic acid, 2-[[[(1S)-1-[(3R,4S)-1-(2-methoxy-2-oxoethyl)-2-oxo-4-phenyl-3-azetidin yl]-3-methylbutyl]amino]carbonyl]-, 2-[(4-nitrophenyl)sulfonyl]ethyl ester, (2S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66646-88-6,120238-40-6,138495-05-3
(E)-N-benzylideneglycine methyl ester

: 482598-88-9
(S)-2-[(S)-1-((3R,4S)-1-Methoxycarbonylmethyl-2-oxo-4-phenyl-azetidin-3-yl)-3-methyl-butylcarbamoyl]-pyrrolidine-1-carboxylic acid 2-(4-nitro-benzenesulfonyl)-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 1.5 h / -30 °C / Irradiation

2: HNEt₂ / tetrahydrofuran / 4.5 h / 20 °C

3: tetrahydrofuran / 2 h / 20 °C

With diethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1002/1099-0690(200208)2002:16<2686::AID-EJOC2686>3.0.CO;2-1

Reference yield:

: 193954-24-4
(S)-(9H-fluoren-9-yl)methyl (1-diazo-5-methyl-2-oxohexan-3-yl)carbamate

: 482598-88-9
(S)-2-[(S)-1-((3R,4S)-1-Methoxycarbonylmethyl-2-oxo-4-phenyl-azetidin-3-yl)-3-methyl-butylcarbamoyl]-pyrrolidine-1-carboxylic acid 2-(4-nitro-benzenesulfonyl)-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 1.5 h / -30 °C / Irradiation

2: HNEt₂ / tetrahydrofuran / 4.5 h / 20 °C

3: tetrahydrofuran / 2 h / 20 °C

With diethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1002/1099-0690(200208)2002:16<2686::AID-EJOC2686>3.0.CO;2-1

Reference yield:

: 482598-86-7
{(3R,4S)-3-[(S)-1-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyl]-2-oxo-4-phenyl-azetidin-1-yl}-acetic acid methyl ester

: 482598-88-9
(S)-2-[(S)-1-((3R,4S)-1-Methoxycarbonylmethyl-2-oxo-4-phenyl-azetidin-3-yl)-3-methyl-butylcarbamoyl]-pyrrolidine-1-carboxylic acid 2-(4-nitro-benzenesulfonyl)-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: HNEt₂ / tetrahydrofuran / 4.5 h / 20 °C

2: tetrahydrofuran / 2 h / 20 °C

With diethylamine; In tetrahydrofuran;
DOI:10.1002/1099-0690(200208)2002:16<2686::AID-EJOC2686>3.0.CO;2-1