9-(tert-butoxycarbonyl)-9-azabicyclo[4.2.1]nonane-2-carboxylic acid

Base Information

Chemical Name:9-(tert-butoxycarbonyl)-9-azabicyclo[4.2.1]nonane-2-carboxylic acid
CAS No.:125736-05-2
Molecular Formula:C₁₄H₂₃NO₄
Molecular Weight:269.341
Hs Code.:
Mol file:125736-05-2.mol

Synonyms:9-Azabicyclo[4.2.1]nonane-2,9-dicarboxylicacid, 9-(1,1-dimethylethyl) ester, endo- (9CI);9-Azabicyclo[4.2.1]nonane-2,9-dicarboxylic acid, 9-(1,1-dimethylethyl) ester,endo-(?à)-

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Chemical Property of 9-(tert-butoxycarbonyl)-9-azabicyclo[4.2.1]nonane-2-carboxylic acid

Chemical Property:

Vapor Pressure:1.51E-07mmHg at 25°C
Boiling Point:400.9°C at 760 mmHg
Flash Point:196.2°C
Density:1.165g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 9-(tert-butoxycarbonyl)-9-azabicyclo[4.2.1]nonane-2-carboxylic acid

There total 5 articles about 9-(tert-butoxycarbonyl)-9-azabicyclo[4.2.1]nonane-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 125736-06-3,125736-07-4,129099-02-1,129170-27-0
(1R,2R)- and (1R,2S)-9-(tert-butoxycarbonyl)-2-(methoxycarbonyl)-9-azabicyclo<4.2.1>nonane

: 125736-03-0,125736-05-2,129099-03-2,129099-04-3
(R)-9-Aza-bicyclo[4.2.1]nonane-2,9-dicarboxylic acid 9-tert-butyl ester

Guidance literature:: With potassium hydroxide; water; In methanol; for 20h; Ambient temperature;
DOI:10.1021/jo00304a012

Reference yield:

: 129001-05-4,129099-01-0
C₁₇H₂₇NO₄S₂

: 125736-03-0,125736-05-2,129099-03-2,129099-04-3
(R)-9-Aza-bicyclo[4.2.1]nonane-2,9-dicarboxylic acid 9-tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / W-2 Raney-Ni / ethanol / 0.5 h / Heating

2: 98 percent / potassium hydroxide, H₂O / methanol / 20 h / Ambient temperature

With potassium hydroxide; W-2 Raney-Ni; water; In methanol; ethanol;
DOI:10.1021/jo00304a012