Carbonic acid, 3-(2-methoxyphenyl)-2-propenyl methyl ester

Base Information

Chemical Name:Carbonic acid, 3-(2-methoxyphenyl)-2-propenyl methyl ester
CAS No.:488151-82-2
Molecular Formula:C12H14O4
Molecular Weight:222.241
Hs Code.:

Synonyms:

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Chemical Property of Carbonic acid, 3-(2-methoxyphenyl)-2-propenyl methyl ester

Chemical Property:

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Technology Process of Carbonic acid, 3-(2-methoxyphenyl)-2-propenyl methyl ester

There total 2 articles about Carbonic acid, 3-(2-methoxyphenyl)-2-propenyl methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1504-61-6
2-methoxycinnamyl alcohol

: 79-22-1
methyl chloroformate

: 488151-82-2
2-methoxycinnamyl methyl carbonate

Guidance literature:: 2-methoxycinnamyl alcohol; With pyridine; dmap; In dichloromethane; at 0 ℃; for 0.333333h;

methyl chloroformate; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/acs.joc.0c01683

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 488151-82-2
2-methoxycinnamyl methyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.33 h / 0 °C

1.2: 0 - 20 °C

1.3: -78 - 20 °C

2.1: dmap; pyridine / dichloromethane / 0.33 h / 0 °C

2.2: 0 - 20 °C

With pyridine; dmap; sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/acs.joc.0c01683

Reference yield: 99.0%

: 488151-82-2
2-methoxycinnamyl methyl carbonate

: 18424-76-5
sodiodimethylmalonate

: C₁₅H₁₈O₅

Guidance literature:: With propylamine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₀H₂₄NO₂P; In tetrahydrofuran; at 20 ℃; for 1h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja210923k