1-(5-(4-Ethylphenyl)-2-thienyl)ethanone O-butyloxime

Base Information

Chemical Name:1-(5-(4-Ethylphenyl)-2-thienyl)ethanone O-butyloxime
CAS No.:93599-14-5
Molecular Formula:C18H23NOS
Molecular Weight:301.4463
Hs Code.:

Synonyms:BRN 4452921;1-(5-(4-Ethylphenyl)-2-thienyl)ethanone O-butyloxime;ETHANONE, 1-(5-(4-ETHYLPHENYL)-2-THIENYL)-, O-BUTYLOXIME;93599-14-5;LS-67424

Suppliers and Price of 1-(5-(4-Ethylphenyl)-2-thienyl)ethanone O-butyloxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1-(5-(4-Ethylphenyl)-2-thienyl)ethanone O-butyloxime

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:416.645°C at 760 mmHg
Flash Point:205.78°C
Density:1.045g/cm³
XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:301.15003553
Heavy Atom Count:21
Complexity:323

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCON=C(C)C1=CC=C(S1)C2=CC=C(C=C2)CC
Isomeric SMILES:CCCCO/N=C(\C)/C1=CC=C(S1)C2=CC=C(C=C2)CC

Technology Process of 1-(5-(4-Ethylphenyl)-2-thienyl)ethanone O-butyloxime

There total 5 articles about 1-(5-(4-Ethylphenyl)-2-thienyl)ethanone O-butyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 109-69-3
n-Butyl chloride

: 93599-32-7
1-[5-(4-Ethyl-phenyl)-thiophen-2-yl]-ethanone oxime

: 93599-14-5
1-[5-(4-Ethyl-phenyl)-thiophen-2-yl]-ethanone O-butyl-oxime

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; for 1h; Ambient temperature;

Reference yield:

: 88-15-3,97511-16-5
2-Acetylthiophene

: 93599-14-5
1-[5-(4-Ethyl-phenyl)-thiophen-2-yl]-ethanone O-butyl-oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 32 percent / aq. CuCl₂*2H₂O, 18-crown-6 / a) 0-5 deg C, 1 h b) room temperature, 4 h

2: 85 percent / hydroxylamine hydrochloride, pyridine / ethanol / 5 h / Heating

3: 55 percent / 30percent aq. NaOH / tetrabutylammonium hydrogen sulphate / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; sodium hydroxide; 18-crown-6 ether; hydroxylamine hydrochloride; tetra(n-butyl)ammonium hydrogensulfate; In ethanol; dichloromethane;

Reference yield:

: 93599-28-1
1-[5-(4-ethylphenyl)thiophen-2-yl]ethan-1-one

: 93599-14-5
1-[5-(4-Ethyl-phenyl)-thiophen-2-yl]-ethanone O-butyl-oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / hydroxylamine hydrochloride, pyridine / ethanol / 5 h / Heating

2: 55 percent / 30percent aq. NaOH / tetrabutylammonium hydrogen sulphate / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; sodium hydroxide; hydroxylamine hydrochloride; tetra(n-butyl)ammonium hydrogensulfate; In ethanol; dichloromethane;