Pyrazino[2,3-b]quinoxalin-2-amine, 3,4-dihydro-3-imino-N,4-bis(4-methylphenyl)-

Base Information

Chemical Name:Pyrazino[2,3-b]quinoxalin-2-amine, 3,4-dihydro-3-imino-N,4-bis(4-methylphenyl)-
CAS No.:489430-90-2
Molecular Formula:C₂₄H₂₀N₆
Molecular Weight:392.463
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pyrazino[2,3-b]quinoxalin-2-amine, 3,4-dihydro-3-imino-N,4-bis(4-methylphenyl)-

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Technology Process of Pyrazino[2,3-b]quinoxalin-2-amine, 3,4-dihydro-3-imino-N,4-bis(4-methylphenyl)-

There total 1 articles about Pyrazino[2,3-b]quinoxalin-2-amine, 3,4-dihydro-3-imino-N,4-bis(4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 2213-63-0
2,3-dichloroquinoxaline

: 1637785-11-5
C₁₆H₁₈N₄

: 489430-90-2
(3-imino-4-p-tolyl-3,4-dihydro-pyrazino[2,3-b]quinoxalin-2-yl)-p-tolyl-amine

Guidance literature:: In ethanol; Heating;
DOI:10.1515/znb-2002-0816

Reference yield: 10.0%

: 2078-54-8
2,6-diisopropylphenol

: 557-20-0
diethylzinc

: 489430-90-2
(3-imino-4-p-tolyl-3,4-dihydro-pyrazino[2,3-b]quinoxalin-2-yl)-p-tolyl-amine

: [Zn(2,6-diisopropylphenolate)(3-imino-4-p-tolyl-3,4-dihydro-pyrazino[2,3-b]-quinoxaline-2-yl)-p-tolyl-amine^(1-))]6

Guidance literature:: In tetrahydrofuran; toluene; manipulations under Ar atmosphere; soln. of Zn compd. in toluene dissolved in THF, treated with excess of phenol deriv., stirred for 30 min, soln. of quinoxaline deriv. in THF added, suspn. stirred until dissolved (3-4 h); isolated, elem. anal.;
DOI:10.1515/znb-2002-0816