Thieno[2,3-c]pyridine-3,6(5H)-dicarboxylic acid, 2-[[[(2-chlorophenyl)amino]thioxomethyl]amino]-4,7-dihydro-, diethyl ester

Base Information

Chemical Name:Thieno[2,3-c]pyridine-3,6(5H)-dicarboxylic acid, 2-[[[(2-chlorophenyl)amino]thioxomethyl]amino]-4,7-dihydro-, diethyl ester
CAS No.:491602-24-5
Molecular Formula:C₂₀H₂₂ClN₃O₄S₂
Molecular Weight:467.997
Hs Code.:
Mol file:491602-24-5.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Thieno[2,3-c]pyridine-3,6(5H)-dicarboxylic acid, 2-[[[(2-chlorophenyl)amino]thioxomethyl]amino]-4,7-dihydro-, diethyl ester

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Technology Process of Thieno[2,3-c]pyridine-3,6(5H)-dicarboxylic acid, 2-[[[(2-chlorophenyl)amino]thioxomethyl]amino]-4,7-dihydro-, diethyl ester

There total 1 articles about Thieno[2,3-c]pyridine-3,6(5H)-dicarboxylic acid, 2-[[[(2-chlorophenyl)amino]thioxomethyl]amino]-4,7-dihydro-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.9%

: 95-51-2
o-chloroaniline

: 258330-01-7
diethyl 2-isothiocyanato-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,6-dicarboxylate

: 491602-24-5
diethyl 2-({[(o-chlorophenyl)amino]carbothioyl}amino)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,6-dicarboxylate

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1080/10426500211720

Reference yield: 68.3%

: 491602-24-5
diethyl 2-({[(o-chlorophenyl)amino]carbothioyl}amino)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,6-dicarboxylate

: 491602-33-6
ethyl 3-amino-2-o-chlorophenylamino-4-oxo-3,5,6,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidine-7(4H)-carboxylate

Guidance literature:: With hydrazine hydrate; In ethanol; Heating;
DOI:10.1080/10426500211720

Reference yield:

: 491602-24-5
diethyl 2-({[(o-chlorophenyl)amino]carbothioyl}amino)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3,6-dicarboxylate

: ethyl 3-o-chlorophenyl-10-oxo-6,8,9,10-tetrahydropyrido[4',3':4,5]thieno[2,3-d][1,2,4]triazolo[1,5-a]pyrimidine-7-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 68.3 percent / hydrazine hydrate / ethanol / Heating

2: 59.6 percent / p-TSA / Heating

With toluene-4-sulfonic acid; hydrazine hydrate; In ethanol;
DOI:10.1080/10426500211720