3-Butyn-1-ol, 4-(dimethylphenylsilyl)-

Base Information

Chemical Name:3-Butyn-1-ol, 4-(dimethylphenylsilyl)-
CAS No.:492440-09-2
Molecular Formula:C12H16OSi
Molecular Weight:204.344
Hs Code.:
DSSTox Substance ID:DTXSID20468188
Nikkaji Number:J1.859.127H
Wikidata:Q82295306
Mol file:492440-09-2.mol

Synonyms:3-Butyn-1-ol, 4-(dimethylphenylsilyl)-;492440-09-2;DTXSID20468188

Suppliers and Price of 3-Butyn-1-ol, 4-(dimethylphenylsilyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-Butyn-1-ol, 4-(dimethylphenylsilyl)-

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:204.097041664
Heavy Atom Count:14
Complexity:227

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C#CCCO)C1=CC=CC=C1

Technology Process of 3-Butyn-1-ol, 4-(dimethylphenylsilyl)-

There total 1 articles about 3-Butyn-1-ol, 4-(dimethylphenylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 768-33-2
phenyldimethylsilyl chloride

: 927-74-2
3-Butyn-1-ol

: 492440-09-2
4-(dimethyl(phenyl)silyl)but-3-yn-1-ol

Guidance literature:: 3-Butyn-1-ol; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 0.333333h;

phenyldimethylsilyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 4h;
DOI:10.1021/ja060812g

Reference yield: 91.0%

: 492440-09-2
4-(dimethyl(phenyl)silyl)but-3-yn-1-ol

: 104066-56-0
3-(dimethyl(phenyl)silyl)but-3-en-1-ol

Guidance literature:: With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; hydrogen; In chloroform; at 20 ℃; for 12h; under 7500.75 Torr; Autoclave;
DOI:10.1021/jacs.9b09658

Reference yield: 75.0%

: 40742-21-0
1‐(but‐3‐en‐1‐yloxy)‐4‐nitrobenzene

: 492440-09-2
4-(dimethyl(phenyl)silyl)but-3-yn-1-ol

: 492440-10-5
(E)-3-[1-(Dimethyl-phenyl-silanyl)-meth-(Z)-ylidene]-7-(4-nitro-phenoxy)-hept-5-en-1-ol

Guidance literature:: With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; In acetone; at 20 ℃;
DOI:10.1002/anie.200290019