1-Pyrrolidineheptanoic acid, 2-[(1E,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[3-(methoxymethyl) phenyl]-1-butenyl]-5-oxo-, (2R)-

Base Information

• Chemical Name: 1-Pyrrolidineheptanoic acid, 2-[(1E,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[3-(methoxymethyl) phenyl]-1-butenyl]-5-oxo-, (2R)-
• CAS No.: 494224-26-9
• Molecular Formula: C29H47NO5Si
• Molecular Weight: 517.77300
• Mol file: 494224-26-9.mol

Synonyms:

Chemical Property of 1-Pyrrolidineheptanoic acid, 2-[(1E,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[3-(methoxymethyl) phenyl]-1-butenyl]-5-oxo-, (2R)-

Chemical Property:

• Boiling Point: 625.3±55.0 °C(Predicted)
• PSA: 76.07000
• Density: 1.067±0.06 g/cm3(Predicted)
• LogP: 6.28610

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Pyrrolidineheptanoic acid, 2-[(1E,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[3-(methoxymethyl) phenyl]-1-butenyl]-5-oxo-, (2R)-

There total 1 articles about 1-Pyrrolidineheptanoic acid, 2-[(1E,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[3-(methoxymethyl) phenyl]-1-butenyl]-5-oxo-, (2R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(15α,13E)-9-oxo-15-(t-butyldimethylsilyloxy)-16-(3-methoxymethylphenyl)-17,18,19,20-tetranor-8-azaprost-13-enoic acid ethyl ester (494224-25-8) → (15α,13E)-9-oxo-15-(t-butyldimethylsilyloxy)-16-(3-methoxymethylphenyl)-17,18,19,20-tetranor-8-azaprost-13-enoic acid (494224-26-9)

Guidance literature:

With sodium hydroxide; water; In tetrahydrofuran; methanol; for 2h;

Reference yield:

(15α,13E)-9-oxo-15-(t-butyldimethylsilyloxy)-16-(3-methoxymethylphenyl)-17,18,19,20-tetranor-8-azaprost-13-enoic acid (494224-26-9) + methanesulfonamide (3144-09-0) → (15α,13E)-9-oxo-15-(t-butyldimethylsilyloxy)-16-(3-methoxymethylphenyl)-17,18,19,20-tetranor-8-azaprost-13-enoic acid N-mesylamide (494224-27-0)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

upstream raw materials:

(15α,13E)-9-oxo-15-(t-butyldimethylsilyloxy)-16-(3-methoxymethylphenyl)-17,18,19,20-tetranor-8-azaprost-13-enoic acid ethyl ester

Downstream raw materials:

(15α,13E)-9-oxo-15-(t-butyldimethylsilyloxy)-16-(3-methoxymethylphenyl)-17,18,19,20-tetranor-8-azaprost-13-enoic acid N-mesylamide

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