Dimethyldichloroplumbane

Base Information

• Chemical Name: Dimethyldichloroplumbane
• CAS No.: 1520-77-0
• Molecular Formula: C2H6 Cl2 Pb
• Molecular Weight: 308.176
• Mol file: 1520-77-0.mol

Synonyms:Dimethylleaddichloride (6CI); Lead, dichlorodimethyl- (7CI); Dichlorodimethyllead;Dichlorodimethylplumbane; Dimethyldichlorolead; Dimethyldichloroplumbane;Dimethylead dichloride

Chemical Property of Dimethyldichloroplumbane

Chemical Property:

• Vapor Pressure: 5.42mmHg at 25°C
• Boiling Point: 148.2°C at 760 mmHg
• Flash Point: 43.4°C
• PSA: 0.00000
• LogP: -5.10060

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dimethyldichloroplumbane

There total 1 articles about Dimethyldichloroplumbane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trimethyllead chloride (1520-78-1) → dimethyllead dichloride (1520-77-0) + Tetramethylblei-(IV) (75-74-1)

Guidance literature:

In chloroform-d1; 70°C, 24 h;

Reference yield: 70.0%

diacetylbis(4-methoxybenzoylhydrazone) + dimethyllead dichloride (1520-77-0) → Pb(CH3OC6H4CONNC(CH3)C(CH3)NNCOC6H4OCH3)(CH3)2

Guidance literature:

With NaH; In tetrahydrofuran; methanol; refluxing a mixt. of NaH, hydrazone and (CH3)2PbCl2 in THF/CH3OH for 3 h;; filtration; pptn. from concd. filtrate on cooling to -20°C; elem. anal.;;

Reference yield: 65.0%

[Co(C10N4H12(CH3)4)(CH3)2](1+)*ClO4(1-)*H2O=[Co(C10N4H12(CH3)4)(CH3)2]ClO4*H2O + dimethyllead dichloride (1520-77-0) → Tetramethylblei-(IV) (75-74-1)

Guidance literature:

In water; byproducts: CH4; reaction was carried out in the dark at room temp. in aq. soln. contg. 0.1 M KCl; product was identified by MAS;

DOI:10.1016/S0020-1693(00)82348-8

upstream raw materials:

trimethyllead chloride

Downstream raw materials:

Tetramethylblei-(IV)

[PtCl(PbMe₂Cl)(6-methylpyridine-2-phenylimine)(dimethyl maleate)]

Refernces