6-(Hydroxyiminomethyl)pyridine-2-carbothioamide

Base Information

Chemical Name:6-(Hydroxyiminomethyl)pyridine-2-carbothioamide
CAS No.:78797-09-8
Molecular Formula:C₇H₇N₃OS
Molecular Weight:181.218
Hs Code.:
DSSTox Substance ID:DTXSID101000024
Mol file:78797-09-8.mol

Synonyms:78797-09-8;DTXSID101000024;6-[(Hydroxyimino)methyl]pyridine-2-carboximidothioic acid

Suppliers and Price of 6-(Hydroxyiminomethyl)pyridine-2-carbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 6-(Hydroxyiminomethyl)pyridine-2-carbothioamide

Chemical Property:

Vapor Pressure:0.00448mmHg at 25°C
Boiling Point:277.6°C at 760 mmHg
Flash Point:121.7°C
PSA：103.59000
Density:1.4g/cm³
LogP:1.22420
XLogP3:0.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:181.03098303
Heavy Atom Count:12
Complexity:195

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=NC(=C1)C(=S)N)C=NO

Technology Process of 6-(Hydroxyiminomethyl)pyridine-2-carbothioamide

There total 2 articles about 6-(Hydroxyiminomethyl)pyridine-2-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 78797-07-6
6-(diacetoxymethyl)pyridine-2-carbothioamide

: 78797-09-8
6-formylpyridine-2-carbothioamide oxime

Guidance literature:: With hydroxylamine hydrochloride; In ethanol; for 0.5h; Heating;
DOI:10.1021/jm00142a012

Reference yield:

: 78797-06-5
2-cyano-6-(diacetoxymethyl)pyridine

: 78797-09-8
6-formylpyridine-2-carbothioamide oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / (C₂H₅)3N, pyridine, H₂S / 1 h

2: 76 percent / NH₂OH*HCl / ethanol / 0.5 h / Heating

With pyridine; hydrogen sulfide; hydroxylamine hydrochloride; triethylamine; In ethanol;
DOI:10.1021/jm00142a012