Senkyunolide S

Base Information

• Chemical Name: Senkyunolide S
• CAS No.: 172723-28-3
• Molecular Formula: C12H16O5
• Molecular Weight: 240.25

Synonyms:1(3H)-Isobenzofuranone, 4,5,6,7-tetrahydro-6,7-dihydroxy-3-(2-hydroxybutylidene)-, [3Z(R*),6α,7β]-;1(3H)-Isobenzofuranone, 4,5,6,7-tetrahydro-6,7-dihydroxy-3-[(2R)-2-hydroxybutylidene]-, (3Z,6R,7R)-rel-;rel-(3Z,6R,7R)-4,5,6,7-Tetrahydro-6,7-dihydroxy-3-[(2R)-2-hydroxybutylidene]-1(3H)-isobenzofuranone;

Chemical Property of Senkyunolide S

Chemical Property:

• PSA: 86.99000
• LogP: 0.01020

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Senkyunolide S

There total 2 articles about Senkyunolide S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

senkyunolide E (102848-87-3,94530-84-4) → (6S,7S)-6,7-Dihydroxy-3-[(R)-2-hydroxy-but-(Z)-ylidene]-4,5,6,7-tetrahydro-3H-isobenzofuran-1-one (172549-37-0,172723-28-3) + (6S,7S)-6,7-Dihydroxy-3-[(S)-2-hydroxy-but-(Z)-ylidene]-4,5,6,7-tetrahydro-3H-isobenzofuran-1-one (172723-28-3)

Guidance literature:

With sulfuric acid; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, RT, 30 min, 2.) dioxane, water, 0 deg C, 1 h;

DOI:10.1016/0031-9422(95)00524-2

Reference yield:

senkyunolide E (102848-87-3,94530-84-4) → (6S,7S)-6,7-Dihydroxy-3-[(R)-2-hydroxy-but-(Z)-ylidene]-4,5,6,7-tetrahydro-3H-isobenzofuran-1-one (172549-37-0,172723-28-3) + (6S,7S)-6,7-Dihydroxy-3-[(S)-2-hydroxy-but-(Z)-ylidene]-4,5,6,7-tetrahydro-3H-isobenzofuran-1-one (172723-28-3)

Guidance literature:

With sulfuric acid; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, RT, 30 min, 2.) dioxane, water, 0 deg C, 1 h;

DOI:10.1016/0031-9422(95)00524-2

upstream raw materials:

senkyunolide E

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