Technology Process of (4S,15R)-15α,16-Epoxykaurane-7β,17,19-triol
There total 7 articles about (4S,15R)-15α,16-Epoxykaurane-7β,17,19-triol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 290 mg / SeO2 / dioxane; H2O / 9 h / Ambient temperature
2: pyridine
3: 390 mg / 5percent KOH / methanol / 24 h / Ambient temperature
4: ethanol / 48 h / 25 °C / Gibberella fujikuroi (ACC 917), AMO 1618
With
pyridine; potassium hydroxide; selenium(IV) oxide;
In
1,4-dioxane; methanol; ethanol; water;
DOI:10.1016/0031-9422(91)85102-6
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 305 mg / SeO2, t-butyl hydroperoxide / CH2Cl2 / 8 h / Ambient temperature
2: ethanol / 48 h / 25 °C / Gibberella fujikuroi (ACC 917), AMO 1618
With
tert.-butylhydroperoxide; selenium(IV) oxide;
In
ethanol; dichloromethane;
DOI:10.1016/0031-9422(91)85102-6
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine
2: 390 mg / 5percent KOH / methanol / 24 h / Ambient temperature
3: ethanol / 48 h / 25 °C / Gibberella fujikuroi (ACC 917), AMO 1618
With
pyridine; potassium hydroxide;
In
methanol; ethanol;
DOI:10.1016/0031-9422(91)85102-6