2,4-Dicyano-3-methyl-3-propylglutarimide

Base Information

Chemical Name:2,4-Dicyano-3-methyl-3-propylglutarimide
CAS No.:64635-91-2
Molecular Formula:C₁₁H₁₃N₃O₂
Molecular Weight:219.243
Hs Code.:
NSC Number:39835
DSSTox Substance ID:DTXSID10983239
ChEMBL ID:CHEMBL1900728

Synonyms:64635-91-2;MLS002608187;2,4-Dicyano-3-methyl-3-propylglutarimide;BRN 0018642;Glutarimide, 2,4-dicyano-3-methyl-3-propyl-;NSC39835;3,5-Piperidinedicarbonitrile, 2,6-dioxo-4-methyl-4-propyl-;SCHEMBL5856469;CHEMBL1900728;DTXSID10983239;QZTFQQBYBVMLFQ-UHFFFAOYSA-N;HMS3078N04;NSC 39835;NSC-39835;SMR001526938;4-Methyl-2,6-dioxo-4-propyl-piperidine-3,5-dicarbonitrile;6-Hydroxy-4-methyl-2-oxo-4-propyl-2,3,4,5-tetrahydropyridine-3,5-dicarbonitrile

Suppliers and Price of 2,4-Dicyano-3-methyl-3-propylglutarimide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2,4-Dicyano-3-methyl-3-propylglutarimide

Chemical Property:

Vapor Pressure:1.43E-09mmHg at 25°C
Boiling Point:485.3°C at 760 mmHg
Flash Point:247.3°C
Density:1.19g/cm³
XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:219.100776666
Heavy Atom Count:16
Complexity:389

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC1(C(C(=O)NC(=O)C1C#N)C#N)C

Technology Process of 2,4-Dicyano-3-methyl-3-propylglutarimide

There total 4 articles about 2,4-Dicyano-3-methyl-3-propylglutarimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 107-87-9
2-Pentanone

: 105-56-6
ethyl 2-cyanoacetate

: 64635-91-2
4-methyl-2,6-dioxo-4-propylpiperidine-3,5-dicarbonitrile

Guidance literature:: With methanol; ammonia; In ethanol; at 20 ℃; for 168h;
DOI:10.1002/anie.200700632

Reference yield:

: 107-87-9
2-Pentanone

: 64635-91-2
4-methyl-2,6-dioxo-4-propylpiperidine-3,5-dicarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate, acetic acid / benzene / 45 h / Heating

2: 1.) Na, C₂H₅OH / 1.) reflux, 15 min, 2.) overnight

With ammonium acetate; ethanol; sodium; acetic acid; In benzene;
DOI:10.1021/jo00347a013