2-Methyl-9-aminoellipticinium acetate

Base Information

• Chemical Name: 2-Methyl-9-aminoellipticinium acetate
• CAS No.: 148528-69-2
• Mol file: 148528-69-2.mol

Synonyms:

Chemical Property of 2-Methyl-9-aminoellipticinium acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Methyl-9-aminoellipticinium acetate

There total 5 articles about 2-Methyl-9-aminoellipticinium acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

Acetate9-acetylamino-2,5,11-trimethyl-6H-pyrido[4,3-b]carbazol-2-ium; (148528-68-1) → 2-methyl-9-aminoellipticinium acetate (148528-69-2)

Guidance literature:

With hydrogenchloride; for 4h; Heating;

Reference yield:

9-bromoellipticine (18073-34-2) → 2-methyl-9-aminoellipticinium acetate (148528-69-2)

Guidance literature:

Multi-step reaction with 5 steps

1: 50 percent / 33percent aq. NH₃, Cu, CuCl / 36 h / 170 °C

2: 92 percent / pyridine / 3 h

3: 96 percent / dimethylformamide / 4 h

4: 84 percent / anion resin exchange column in the acetate form / dimethylformamide; H₂O

5: 74 percent / 1.2N aq. HCl / 4 h / Heating

With pyridine; hydrogenchloride; ammonium hydroxide; anion resin exchange column in the acetate form; copper; copper(l) chloride; In water; N,N-dimethyl-formamide;

Reference yield:

9-Acetylamino-2,5,11-trimethyl-6H-pyrido[4,3-b]carbazol-2-ium; iodide → 2-methyl-9-aminoellipticinium acetate (148528-69-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 84 percent / anion resin exchange column in the acetate form / dimethylformamide; H₂O

2: 74 percent / 1.2N aq. HCl / 4 h / Heating

With hydrogenchloride; anion resin exchange column in the acetate form; In water; N,N-dimethyl-formamide;

upstream raw materials:

Acetate₉-acetylamino-2,5,11-trimethyl-6H-pyrido[4,3-b]carbazol-2-ium;

9-bromoellipticine

9-acetylaminoellipticine

9-aminoellipticine