Acetic acid, ((7-amino-(1,2,4)triazolo(1,5-c)pyrimidin-5-yl)thio)-, (2-bromo-3-phenyl-2-propenylidene)hydrazide

Base Information

Chemical Name:Acetic acid, ((7-amino-(1,2,4)triazolo(1,5-c)pyrimidin-5-yl)thio)-, (2-bromo-3-phenyl-2-propenylidene)hydrazide
CAS No.:143212-87-7
Molecular Formula:C₁₆H₁₄BrN₇OS
Molecular Weight:432.303
Hs Code.:

Synonyms:BRN 5833540;143212-87-7;Acetic acid, ((7-amino-(1,2,4)triazolo(1,5-c)pyrimidin-5-yl)thio)-, (2-bromo-3-phenyl-2-propenylidene)hydrazide;2-[(7-Amino-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)sulfanyl]-N-[(E)-[(Z)-2-bromo-3-phenylprop-2-enylidene]amino]acetamide;NSC676856;C16H14BrN7OS;C16-H14-Br-N7-O-S;STL445895;AKOS005220635;2-[(7-amino-[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)sulfanyl]-N-[(E)-[(Z)-2-bromo-3-phenyl-prop-2-enylidene]amino]acetamide;2-[(7-amino[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)sulfanyl]-N'-[(1E,2Z)-2-bromo-3-phenylprop-2-en-1-ylidene]acetohydrazide;2-[(7-Amino[1,2,4]triazolo[1,5-c]pyrimidin-5-yl)thio]- N'-[(1E,2Z)-2-bromo-3-phenylprop-2-en-1-ylidene]acetohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid, ((7-amino-(1,2,4)triazolo(1,5-c)pyrimidin-5-yl)thio)-, (2-bromo-3-phenyl-2-propenylidene)hydrazide

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:6
Exact Mass:431.01639
Heavy Atom Count:26
Complexity:541

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=C(C=NNC(=O)CSC2=NC(=CC3=NC=NN32)N)Br
Isomeric SMILES:C1=CC=C(C=C1)/C=C(/C=N/NC(=O)CSC2=NC(=CC3=NC=NN32)N)\Br

Technology Process of Acetic acid, ((7-amino-(1,2,4)triazolo(1,5-c)pyrimidin-5-yl)thio)-, (2-bromo-3-phenyl-2-propenylidene)hydrazide

There total 3 articles about Acetic acid, ((7-amino-(1,2,4)triazolo(1,5-c)pyrimidin-5-yl)thio)-, (2-bromo-3-phenyl-2-propenylidene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 5443-49-2
α-bromocinnamaldehyde

: 143212-84-4
(7-amino-s-triazole<1,5-c>yrimidyl-5)thioacetic acid hydrazide

: 143212-87-7
(7-Amino-[1,2,4]triazolo[1,5-c]pyrimidin-5-ylsulfanyl)-acetic acid [(Z)-2-bromo-3-phenyl-prop-2-en-(E)-ylidene]-hydrazide

Guidance literature:: In ethanol; water; for 2h; Heating;
DOI:10.1007/BF00766451

Reference yield:

: 70182-88-6
7-Amino<1,2,4>triazolo<1,5-c>pyrimidine-5(6H)-thione

: 143212-87-7
(7-Amino-[1,2,4]triazolo[1,5-c]pyrimidin-5-ylsulfanyl)-acetic acid [(Z)-2-bromo-3-phenyl-prop-2-en-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / EtONa / ethanol / 3 h / Heating

2: 90 percent / H₂NNH₂ / ethanol; H₂O; diethyl ether / 0.5 h / Ambient temperature

3: 73 percent / ethanol; H₂O / 2 h / Heating

With sodium ethanolate; hydrazine; In diethyl ether; ethanol; water;
DOI:10.1007/BF00766451

Reference yield:

: 143212-80-0
ethyl (7-amino-s-triazole<1,5-c>pyrimidyl-5)thioacetate

: 143212-87-7
(7-Amino-[1,2,4]triazolo[1,5-c]pyrimidin-5-ylsulfanyl)-acetic acid [(Z)-2-bromo-3-phenyl-prop-2-en-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / H₂NNH₂ / ethanol; H₂O; diethyl ether / 0.5 h / Ambient temperature

2: 73 percent / ethanol; H₂O / 2 h / Heating

With hydrazine; In diethyl ether; ethanol; water;
DOI:10.1007/BF00766451