Carbamic acid, [[4-[3-[[2-[methyl(2-naphthalenylsulfonyl)amino]ethyl]amino]-3-oxopropyl] phenyl]methyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [[4-[3-[[2-[methyl(2-naphthalenylsulfonyl)amino]ethyl]amino]-3-oxopropyl] phenyl]methyl]-, 1,1-dimethylethyl ester
CAS No.:496945-62-1
Molecular Formula:C28H35N3O5S
Molecular Weight:525.669
Hs Code.:
Mol file:496945-62-1.mol

Synonyms:

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Chemical Property of Carbamic acid, [[4-[3-[[2-[methyl(2-naphthalenylsulfonyl)amino]ethyl]amino]-3-oxopropyl] phenyl]methyl]-, 1,1-dimethylethyl ester

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Technology Process of Carbamic acid, [[4-[3-[[2-[methyl(2-naphthalenylsulfonyl)amino]ethyl]amino]-3-oxopropyl] phenyl]methyl]-, 1,1-dimethylethyl ester

There total 1 articles about Carbamic acid, [[4-[3-[[2-[methyl(2-naphthalenylsulfonyl)amino]ethyl]amino]-3-oxopropyl] phenyl]methyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(2-aminoethyl)-N methyl-2-naphthalenesulfonamide

: 496945-61-0
lithium 3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propionate

: 496945-62-1
N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propanoyl]amino]ethyl]-N-methyl-2-naphthalenesulfonamide

Guidance literature:: With hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In diethyl ether; dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 496945-62-1
N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propanoyl]amino]ethyl]-N-methyl-2-naphthalenesulfonamide

: N-[2-[N-[3-[4-(aminomethyl)phenyl]propyl]amino]ethyl]-N-methyl-2-naphthalenesulfonamide dihydrochloride

Guidance literature:: N-[2-[N-[3-[4-(N-tert-butoxycarbonylaminomethyl)phenyl]propanoyl]amino]ethyl]-N-methyl-2-naphthalenesulfonamide; With borane-THF; In tetrahydrofuran; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 1h;

With di-tert-butyl dicarbonate; sodium carbonate; In 1,4-dioxane; water; at 40 ℃; for 1h;