2-Benzyloctane

Base Information

• Chemical Name: 2-Benzyloctane
• CAS No.: 49826-80-4
• Molecular Formula: C15H24
• Molecular Weight: 204.356
• Mol file: 49826-80-4.mol

Synonyms:2-methyl-1-phenyl-octane;1-Phenyl-2-methyloctan;(2-methyloctyl)benzene;(2-Methyl-octyl)-benzene;2-Methyl-1-phenyl-octan;2-Benzyloctane;

Chemical Property of 2-Benzyloctane

Chemical Property:

• Boiling Point: 107 - 108 °C (1.7 mmHg)
• PSA: 0.00000
• LogP: 4.83560

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Benzyloctane

There total 11 articles about 2-Benzyloctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

phenylmagnesium bromide (1589-82-8) + 2-bromooctane (557-35-7,60251-57-2) → 4-(2,2-dimethyl-3-phenylpropyl)-1-fluorobenzene (49826-80-4)

Guidance literature:

With silver nitrate; In diethyl ether; at 25 ℃; for 3h; Inert atmosphere;

DOI:10.1021/ol800038a

Reference yield: 62.0%

2-iodooctane (36049-78-2,557-36-8) + benzylmagnesium chloride (6921-34-2) → 4-(2,2-dimethyl-3-phenylpropyl)-1-fluorobenzene (49826-80-4)

Guidance literature:

With 1,3-bis-(diphenylphosphino)propane; CoCl₂; In tetrahydrofuran; at 0 ℃; for 2h;

DOI:10.1002/chem.200400545

Reference yield: 57.0%

benzylzinc chloride-lithium chloride complex + 2-bromooctane (557-35-7,60251-57-2) → 4-(2,2-dimethyl-3-phenylpropyl)-1-fluorobenzene (49826-80-4)

Guidance literature:

With silver trifluoromethanesulfonate; In tetrahydrofuran; acetonitrile; at 25 ℃; Inert atmosphere;

DOI:10.1002/asia.201000068

upstream raw materials:

oct-1-ene

toluene

benzylmagnesium chloride

anthracene

Downstream raw materials:

(+)-3(R)-methylnonanoic acid

(3S)-3-Methylnonanoic acid