(8aS)-Decahydro-7β-(1-hydroxy-1-methylethyl)-1,4aβ-dimethyl-1α,2α,8α-naphthalenetriol

Base Information

• Chemical Name: (8aS)-Decahydro-7β-(1-hydroxy-1-methylethyl)-1,4aβ-dimethyl-1α,2α,8α-naphthalenetriol
• CAS No.: 74841-83-1
• Molecular Formula: C₁₅H₂₈O₄
• Molecular Weight: 272.385
• Mol file: 74841-83-1.mol

Synonyms:(1S,2R,4aS,7R,8S,8aS)-7-(1-Hydroxy-1-methyl-ethyl)-1,4a-dimethyl-decahydro-naphthalene-1,2,8-triol;

Chemical Property of (8aS)-Decahydro-7β-(1-hydroxy-1-methylethyl)-1,4aβ-dimethyl-1α,2α,8α-naphthalenetriol

Chemical Property:

• Melting Point: 185 °C (diethyl ether)
• PSA: 80.92000
• LogP: 1.05640

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (8aS)-Decahydro-7β-(1-hydroxy-1-methylethyl)-1,4aβ-dimethyl-1α,2α,8α-naphthalenetriol

There total 8 articles about (8aS)-Decahydro-7β-(1-hydroxy-1-methylethyl)-1,4aβ-dimethyl-1α,2α,8α-naphthalenetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S,4aS,7R,8S,8aS)-1,8-Dihydroxy-7-(1-hydroxy-1-methyl-ethyl)-1,4a-dimethyl-octahydro-naphthalen-2-one (74799-36-3) → chenopotetraol (74841-83-1) + 3-epichenopotetraol (74799-34-1)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; Yield given;

DOI:10.1016/0040-4020(80)87004-9

Reference yield:

α-chenopodiol (67996-31-0) → chenopotetraol (74841-83-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 130 mg / m-CPB / CH₂Cl₂

2: 88 mg / LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; MCPB; In diethyl ether; dichloromethane;

DOI:10.1016/0040-4020(80)87004-9

Reference yield:

C15H26O4 (74799-41-0) → chenopotetraol (74841-83-1)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1016/0040-4020(80)87004-9

upstream raw materials:

C₁₅H₂₆O₄

(1S,4aS,7R,8S,8aS)-1,8-Dihydroxy-7-(1-hydroxy-1-methyl-ethyl)-1,4a-dimethyl-octahydro-naphthalen-2-one

chenopotetraol⁽³⁾monoacetate

chenopotriol

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