4-CARBAMOYL-2,2,5,5-TETRAMETHYL-3-IMIDAZOLINE-3-OXIDE-1-OXYL

Base Information

Chemical Name:4-CARBAMOYL-2,2,5,5-TETRAMETHYL-3-IMIDAZOLINE-3-OXIDE-1-OXYL
CAS No.:69826-43-3
Molecular Formula:C₈H₁₄N₃O₃
Molecular Weight:200.217
Hs Code.:
Mol file:69826-43-3.mol

Synonyms:4-CARBAMOYL-2,2,5,5-TETRAMETHYL-3-IMIDAZOLINE-3-OXIDE-1-OXYL

Suppliers and Price of 4-CARBAMOYL-2,2,5,5-TETRAMETHYL-3-IMIDAZOLINE-3-OXIDE-1-OXYL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-CARBAMOYL-2,2,5,5-TETRAMETHYL-3-IMIDAZOLINE-3-OXIDE-1-OXYL

Chemical Property:

Vapor Pressure:1.61E-06mmHg at 25°C
Melting Point:184-184.8℃
Boiling Point:370.9°C at 760 mmHg
Flash Point:178.1°C
PSA：101.27000
Density:1.28g/cm³
LogP:0.34810
Storage Temp.:0-6°C

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: S24/25:Avoid contact with skin and eyes.;

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-CARBAMOYL-2,2,5,5-TETRAMETHYL-3-IMIDAZOLINE-3-OXIDE-1-OXYL

There total 4 articles about 4-CARBAMOYL-2,2,5,5-TETRAMETHYL-3-IMIDAZOLINE-3-OXIDE-1-OXYL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 95057-92-4
4-cyano-1,2,2,5,5-pentamethyl-2,5-dihydro-1H-imidazole 3-oxide

: 69826-43-3
4-carbamoyl-2,2,5,5-tetramethyl-3-imidazoline 3-oxide 1-oxyl

Guidance literature:: With sodium tungstate; dihydrogen peroxide; ethylene diamine tetraacetic acid tetrasodium salt; for 72h;
DOI:10.1007/BF00950152

Reference yield:

: 4-chlorooximinomethyl-1,2,2,5,5-pentamethyl-3-imidazoline 3-oxide

: 69826-43-3
4-carbamoyl-2,2,5,5-tetramethyl-3-imidazoline 3-oxide 1-oxyl

Guidance literature:: Multi-step reaction with 2 steps

1: 20 percent / KOH / methanol / 3 h

2: 92 percent / aq. H₂O₂, Na₂WO₄*2H₂O, Trilon B / 72 h

With potassium hydroxide; sodium tungstate; dihydrogen peroxide; ethylene diamine tetraacetic acid tetrasodium salt; In methanol;
DOI:10.1007/BF00950152

Reference yield:

: 102277-04-3
4-azidoximinomethyl-1,2,2,5,5-pentamethyl-3-imidazoline 3-oxide

: 69826-43-3
4-carbamoyl-2,2,5,5-tetramethyl-3-imidazoline 3-oxide 1-oxyl

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 0.5 h / Heating

2: 92 percent / aq. H₂O₂, Na₂WO₄*2H₂O, Trilon B / 72 h

With sodium tungstate; dihydrogen peroxide; ethylene diamine tetraacetic acid tetrasodium salt; In benzene;
DOI:10.1007/BF00950152