1-(2-Chloroethyl)-3-methylpiperidine

Base Information

Chemical Name:1-(2-Chloroethyl)-3-methylpiperidine
CAS No.:10298-11-0
Molecular Formula:C8H16 Cl N
Molecular Weight:161.675
Hs Code.:2933399090
European Community (EC) Number:233-673-6
DSSTox Substance ID:DTXSID00908138
Nikkaji Number:J236.754H
Mol file:10298-11-0.mol

Synonyms:1-(2-Chloroethyl)-3-methylpiperidine;10298-11-0;EINECS 233-673-6;starbld0024211;SCHEMBL11602947;DTXSID00908138;AKOS010542106

Suppliers and Price of 1-(2-Chloroethyl)-3-methylpiperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-(2-Chloroethyl)-3-methylpiperidine

Chemical Property:

Vapor Pressure:0.279mmHg at 25°C
Boiling Point:203.3°Cat760mmHg
Flash Point:76.8°C
PSA：3.24000
Density:0.971g/cm³
LogP:1.89500
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:161.0971272
Heavy Atom Count:10
Complexity:95.3

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCCN(C1)CCCl

Technology Process of 1-(2-Chloroethyl)-3-methylpiperidine

There total 3 articles about 1-(2-Chloroethyl)-3-methylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39123-22-3
1-(2-hydroxyethyl)-3-methylpiperidine

: 10298-11-0
β-(3-methyl-piperidino)-ethyl chloride

Guidance literature:: With dmap; thionyl chloride; In chloroform; for 2h; Ambient temperature;
DOI:10.1002/ardp.19953280705

Reference yield:

: 626-56-2,53152-98-0
3-Methylpiperidine

: 10298-11-0
β-(3-methyl-piperidino)-ethyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / acetonitrile / Ambient temperature

2: SOCl₂, 4-DMAP / CHCl₃ / 2 h / Ambient temperature

With dmap; potassium hydroxide; thionyl chloride; In chloroform; acetonitrile;
DOI:10.1002/ardp.19953280705