Stannane, tributyl[(1E)-4-[(4-methoxyphenyl)methoxy]-1-methyl-1-butenyl]-

Base Information

Chemical Name:Stannane, tributyl[(1E)-4-[(4-methoxyphenyl)methoxy]-1-methyl-1-butenyl]-
CAS No.:500702-35-2
Molecular Formula:C25H44O2Sn
Molecular Weight:495.333
Hs Code.:

Synonyms:

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Chemical Property of Stannane, tributyl[(1E)-4-[(4-methoxyphenyl)methoxy]-1-methyl-1-butenyl]-

Chemical Property:

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Technology Process of Stannane, tributyl[(1E)-4-[(4-methoxyphenyl)methoxy]-1-methyl-1-butenyl]-

There total 1 articles about Stannane, tributyl[(1E)-4-[(4-methoxyphenyl)methoxy]-1-methyl-1-butenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 824-94-2
p-methoxybenzyl chloride

: 651713-92-7,138205-96-6
E-5-hydroxy-2-tri-n-butylstannyl-2-pentene

: 500702-35-2
C₂₅H₄₄O₂Sn

Guidance literature:: E-5-hydroxy-2-tri-n-butylstannyl-2-pentene; With sodium hydride; In dimethyl sulfoxide; at 0 - 20 ℃; for 2h;

p-methoxybenzyl chloride; With tetra-(n-butyl)ammonium iodide; at 20 ℃; for 5h;
DOI:10.1002/ejoc.201402234

Reference yield: 76.0%

: 1639124-60-9
C₂₂H₃₆INO₅S

: 500702-35-2
C₂₅H₄₄O₂Sn

: 1639124-59-6
C₃₅H₅₃NO₇S

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; cesium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h; Reagent/catalyst; diastereoselective reaction;
DOI:10.1002/ejoc.201402234

Reference yield:

: 500702-35-2
C₂₅H₄₄O₂Sn

: 1639124-58-5
(5R,7E,9E)-5-hydroxy-12-[(4-methoxyphenyl)methoxy]-5,9-dimethyldodeca-7,9-dien-2-yn-4-one

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; cesium fluoride / N,N-dimethyl-formamide / 1.5 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 20 - 80 °C

3: pyridine-SO₃ complex; pyridine; triethylamine / dichloromethane; dimethyl sulfoxide / 0.5 h / 0 - 20 °C

4: tetrahydrofuran; diethyl ether / 1 h / -30 °C

5: pyridine-SO₃ complex; pyridine; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 - 20 °C

With pyridine; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; pyridine-SO₃ complex; triethylamine; cesium fluoride; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; 1: |Stille Cross Coupling / 3: |Parikh-Doering Oxidation / 5: |Parikh-Doering Oxidation;
DOI:10.1002/ejoc.201402234