4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(3-nitrophenoxy)-

Base Information

Chemical Name:4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(3-nitrophenoxy)-
CAS No.:137988-19-3
Molecular Formula:C₁₇H₁₁NO₇
Molecular Weight:341.277
Hs Code.:
DSSTox Substance ID:DTXSID30160444
Wikidata:Q83028812
Mol file:137988-19-3.mol

Synonyms:BRN 5454009;4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(3-nitrophenoxy)-;7-(Acetyloxy)-3-(3-nitrophenoxy)-4H-1-benzopyran-4-one;137988-19-3;DTXSID30160444;LS-39431

Suppliers and Price of 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(3-nitrophenoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(3-nitrophenoxy)-

Chemical Property:

Vapor Pressure:6.72E-10mmHg at 25°C
Boiling Point:494°Cat760mmHg
Flash Point:211.7°C
Density:1.458g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:341.05355169
Heavy Atom Count:25
Complexity:582

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1=CC2=C(C=C1)C(=O)C(=CO2)OC3=CC=CC(=C3)[N+](=O)[O-]

Technology Process of 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(3-nitrophenoxy)-

There total 4 articles about 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(3-nitrophenoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.7%

: 108-24-7
acetic anhydride

: 137988-03-5
7-Hydroxy-3-(3-nitro-phenoxy)-chromen-4-one

: 137988-19-3
Acetic acid 3-(3-nitro-phenoxy)-4-oxo-4H-chromen-7-yl ester

Guidance literature:: With pyridine; for 0.05h; Heating;
DOI:10.1007/BF00767267

Reference yield:

: 19157-84-7
1-cyanomethyloxy-3-nitrobenzene

: 137988-19-3
Acetic acid 3-(3-nitro-phenoxy)-4-oxo-4H-chromen-7-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) HCl, 2.) zinc chloride, HCl, 3.) water

2: 93.1 percent / boron trifluoride etherate, phosphorus trichloride / 50 - 60 °C

3: 96.7 percent / pyridine / 0.05 h / Heating

With pyridine; hydrogenchloride; boron trifluoride diethyl etherate; water; zinc(II) chloride; phosphorus trichloride;
DOI:10.1007/BF00767267

Reference yield:

: 137987-90-7
1-(2,4-Dihydroxy-phenyl)-2-(3-nitro-phenoxy)-ethanone

: 137988-19-3
Acetic acid 3-(3-nitro-phenoxy)-4-oxo-4H-chromen-7-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93.1 percent / boron trifluoride etherate, phosphorus trichloride / 50 - 60 °C

2: 96.7 percent / pyridine / 0.05 h / Heating

With pyridine; boron trifluoride diethyl etherate; phosphorus trichloride;
DOI:10.1007/BF00767267