5-(3 4-DICHLOROPHENYL)FURFURAL 97

Base Information

• Chemical Name: 5-(3 4-DICHLOROPHENYL)FURFURAL 97
• CAS No.: 52130-34-4
• Molecular Formula: C11H6Cl2O2
• Molecular Weight: 241.073
• Hs Code.: 2932190090
• Mol file: 52130-34-4.mol

Synonyms:5-(3,4-dichlorophenyl)furaldehyde;5-(3,4-dichlorophenyl)-furan-2-yl-carboxaldehyde;5-(3,4-Dichloro-phenyl)-furan-2-carbaldehyde;5-(3,4-Dichlorophenyl)furfural;5-(3,4-dichlorophenyl)-2-furancarbaldehyde;5-(3,4-Dichlorophenyl)-2-furaldehyde;5-(3,4-Dichlorophenyl)furylaldehyde;

Chemical Property of 5-(3 4-DICHLOROPHENYL)FURFURAL 97

Chemical Property:

• Vapor Pressure: 4.57E-06mmHg at 25°C
• Melting Point: 140-143oC(lit.)
• Boiling Point: 382.9°Cat760mmHg
• Flash Point: 185.4°C
• PSA: 30.21000
• Density: 1.392g/cm³
• LogP: 4.06590

Purity/Quality:

98%,99%, ^*data from raw suppliers

5-(3,4-Dichlorophenyl)furfural 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 5-(3 4-DICHLOROPHENYL)FURFURAL 97

There total 6 articles about 5-(3 4-DICHLOROPHENYL)FURFURAL 97 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

5-formylfurane-2-boronic acid (27329-70-0) + 3,4-dichloroiodobenzene (20555-91-3) → 5-(3,4-dichlorophenyl)furfural (52130-34-4)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; In 1,2-dimethoxyethane; ethanol; water; at 65 ℃; for 1h;

DOI:10.1016/j.ejmech.2016.12.024

Reference yield: 80.0%

furfural (98-01-1) + m,p-dichloroaniline (95-76-1) → 5-(3,4-dichlorophenyl)furfural (52130-34-4)

Guidance literature:

With hydrogenchloride; copper dichloride; sodium nitrite; In water; at 0 ℃; for 4h;

DOI:10.1007/s00044-011-9857-0

Reference yield: 57.0%

5-bromo-2-furancarboxaldehyde (1899-24-7) + 3,4-dichlophenylboronic acid (151169-75-4) → 5-(3,4-dichlorophenyl)furfural (52130-34-4)

Guidance literature:

With palladium diacetate; sodium hydrogencarbonate; triphenylphosphine; In ethanol; water; toluene; at 20 - 80 ℃; for 22h;

upstream raw materials:

furfural

m,p-dichloroaniline

4-bromo-1,2-dichlorobenzene

5-bromo-2-furancarboxaldehyde

Downstream raw materials:

2-{[1-[5-(3,4-Dichloro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-4,5-diphenyl-furan-3-carbonitrile

5-(3',4'-dichlorophenyl)furan-2-carbaldehyde oxime

3-[5-(3,4-dichlorophenyl)-2-furyl]acrylic acid

BI-11C3