N,N'-(2-Chlorobenzylidene)bis(2-chlorobenzenemethaneimine)

Base Information

• Chemical Name: N,N'-(2-Chlorobenzylidene)bis(2-chlorobenzenemethaneimine)
• CAS No.: 1498-93-7
• Molecular Formula: C21H15 Cl3 N2
• Molecular Weight: 401.723
• Nikkaji Number: J2.647.757C
• Mol file: 1498-93-7.mol

Synonyms:SCHEMBL8181267;N,N'-(2-Chlorobenzylidene)bis(2-chlorobenzenemethaneimine)

Chemical Property of N,N'-(2-Chlorobenzylidene)bis(2-chlorobenzenemethaneimine)

Chemical Property:

• Boiling Point: 496.7°Cat760mmHg
• Flash Point: 254.2°C
• Density: 1.24g/cm³
• XLogP3: 6.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 400.030082
• Heavy Atom Count: 26
• Complexity: 450

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C=NC(C2=CC=CC=C2Cl)N=CC3=CC=CC=C3Cl)Cl

Technology Process of N,N'-(2-Chlorobenzylidene)bis(2-chlorobenzenemethaneimine)

There total 2 articles about N,N'-(2-Chlorobenzylidene)bis(2-chlorobenzenemethaneimine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-benzaldehyde (89-98-5) → N,N'-Bis<2-chlorobenzylidene>-2-chlorophenylmethanediamine (1498-93-7)

Guidance literature:

With ammonium hydroxide; ethanol;

DOI:10.1021/ja01348a020

Reference yield:

→ N,N'-Bis<2-chlorobenzylidene>-2-chlorophenylmethanediamine (1498-93-7)

Guidance literature:

nach der Meth. v. Hilbert et al., Am. Soc. 54 <1932> 3128: aus 2-Chlor-benzaldehyd;

DOI:10.1039/jr9650003067

Reference yield: 91.0%

N,N'-Bis<2-chlorobenzylidene>-2-chlorophenylmethanediamine (1498-93-7) + C9H18BN → 1-(2-chlorophenyl)but-3-en-1-amine hydrochloride

Guidance literature:

N,N'-Bis<2-chlorobenzylidene>-2-chlorophenylmethanediamine; C₉H₁₈BN; at 40 ℃; for 4h;

With hydrogenchloride; In 1,4-dioxane; water;

DOI:10.1021/acs.orglett.8b01317

upstream raw materials:

2-chloro-benzaldehyde

Downstream raw materials:

2,4,5-tris(2-chlorophenyl)-1H-imidazole

2,4,6-Tris<2-chlorophenyl>-1,3,5-triazabicyclo<3.1.0>hexane

2,5-di(2-chlorophenyl)-3,3,4,4-tetracyanopyrrolidine

bis(2-chlorobenzyl)amine