1-Methyl-3-(N-(4-iodophenylethyl)carbamoyl)-1,4-dihydropyridine

Base Information

Chemical Name:1-Methyl-3-(N-(4-iodophenylethyl)carbamoyl)-1,4-dihydropyridine
CAS No.:97807-23-3
Molecular Formula:C15H17 I N2 O
Molecular Weight:0
Hs Code.:
DSSTox Substance ID:DTXSID40913640
Mol file:97807-23-3.mol

Synonyms:1-methyl-3-(N-(4-iodophenylethyl)carbamoyl)-1,4-dihydropyridine;1-methyl-3-(N-(4-iodophenylethyl)carbamoyl)-1,4-dihydropyridine, 125I-labeled;1-MIECP

Suppliers and Price of 1-Methyl-3-(N-(4-iodophenylethyl)carbamoyl)-1,4-dihydropyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-Methyl-3-(N-(4-iodophenylethyl)carbamoyl)-1,4-dihydropyridine

Chemical Property:

Vapor Pressure:6.12E-10mmHg at 25°C
Boiling Point:495°Cat760mmHg
Flash Point:253.2°C
PSA：32.34000
Density:1.52g/cm³
LogP:3.01180
XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:368.03856
Heavy Atom Count:19
Complexity:384

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C1=CC=C(C=C1)I)NC(=O)C2=CN(C=CC2)C

Technology Process of 1-Methyl-3-(N-(4-iodophenylethyl)carbamoyl)-1,4-dihydropyridine

There total 3 articles about 1-Methyl-3-(N-(4-iodophenylethyl)carbamoyl)-1,4-dihydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 97807-21-1
1-methyl-3-carbamoyl>pyridinium iodide

: 97807-23-3
1-methyl-3-{N-[β-(4-iodophenyl)ethyl]carbamoyl}-1,4-dihydropyridine

Guidance literature:: With sodium dithionite; sodium hydrogencarbonate; In methanol; for 0.166667h;
DOI:10.1021/jm00149a006

Reference yield:

: 97807-20-0
1-methyl-3-ethyl>carbamoyl>pyridinium iodide

: 97807-23-3
1-methyl-3-{N-[β-(4-iodophenyl)ethyl]carbamoyl}-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / sodium iodide, hydrofluoric acid / acetone / 1 h / Ambient temperature

2: 78 percent / sodium dithionite, sodium bicarbonate / methanol / 0.17 h

With sodium dithionite; hydrogen fluoride; sodium hydrogencarbonate; sodium iodide; In methanol; acetone;
DOI:10.1021/jm00149a006

Reference yield:

: 97807-19-7
1-methyl-3-ethyl>carbamoyl>pyridinium iodide

: 97807-23-3
1-methyl-3-{N-[β-(4-iodophenyl)ethyl]carbamoyl}-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide, hydrofluoric acid / acetone / 1 h / Ambient temperature

2: 78 percent / sodium dithionite, sodium bicarbonate / methanol / 0.17 h

With sodium dithionite; hydrogen fluoride; sodium hydrogencarbonate; sodium iodide; In methanol; acetone;
DOI:10.1021/jm00149a006