2-oxo-N-phenylcyclohexanecarboxaMide

Base Information

• Chemical Name: 2-oxo-N-phenylcyclohexanecarboxaMide
• CAS No.: 51089-06-6
• Molecular Formula: C13H15NO2
• Molecular Weight: 217.268
• Mol file: 51089-06-6.mol

Synonyms:2-Oxo-N-phenylcyclohexanecarboxamide;N-Phenyl-cyclohexanon-2-carboxamid;Cyclohexanecarboxamide,2-oxo-N-phenyl;2-Oxo-cyclohexancarbonsaeure-anilid;2-oxo-cyclohexanecarboxylic acid anilide;

Chemical Property of 2-oxo-N-phenylcyclohexanecarboxaMide

Chemical Property:

• PSA: 49.66000
• LogP: 3.03390

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-oxo-N-phenylcyclohexanecarboxaMide

There total 8 articles about 2-oxo-N-phenylcyclohexanecarboxaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2,2-dimethyl-5,6,7,8-tetrahydro-4H-benzo[d][1,3]dioxin-4-one (28637-56-1) + aniline (62-53-3) → 2-oxo-N-phenylcyclohexane-1-carboxamide (51089-06-6)

Guidance literature:

for 0.05h; microwave irradiation;

DOI:10.1016/j.tetlet.2003.08.118

Reference yield: 71.0%

aniline (62-53-3) + ethyl 2-oxocyclohexane carboxylate (1655-07-8) → 2-oxo-N-phenylcyclohexane-1-carboxamide (51089-06-6)

Guidance literature:

at 180 ℃; for 0.5h; Microwave irradiation;

DOI:10.1007/s00894-021-04705-4

Reference yield: 49.0%

2-Oxocyclohexylidenemethanone (132723-22-9) + aniline (62-53-3) → 2-oxo-N-phenylcyclohexane-1-carboxamide (51089-06-6)

Guidance literature:

In 1,3,5-trimethyl-benzene; at 160 ℃; for 1h;

upstream raw materials:

aniline

ethyl 2-oxocyclohexane carboxylate

2-Oxocyclohexylidenemethanone

2,2-dimethyl-5,6,7,8-tetrahydro-4H-benzo[d][1,3]dioxin-4-one

Downstream raw materials:

2-Aminocyclohexen-1-carboxanilid

2-Hydroxy-cyclohexanecarboxylic acid phenylamide

3-amino-1-oxo-2-phenyl-1,2,5,6,7,8-hexahydroisoquinoline-4-carbonitrile

N-phenylcyclohex-1-enecarboxamide

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