2,6-Dinitro-1,1'-biphenyl

Base Information

Chemical Name:2,6-Dinitro-1,1'-biphenyl
CAS No.:5110-81-6
Molecular Formula:C12H8N2O4
Molecular Weight:244.207
Hs Code.:
DSSTox Substance ID:DTXSID10500162
Nikkaji Number:J2.302.621J
Wikidata:Q82351563
Mol file:5110-81-6.mol

Synonyms:5110-81-6;2,6-Dinitro-1,1'-biphenyl;DTXSID10500162

Suppliers and Price of 2,6-Dinitro-1,1'-biphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,6-Dinitro-1,1'-biphenyl

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:244.04840674
Heavy Atom Count:18
Complexity:295

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(C=CC=C2[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 2,6-Dinitro-1,1'-biphenyl

There total 1 articles about 2,6-Dinitro-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 2,6-dinitrobenzenediazonium o-benzenedisulfonimide

: 3958-47-2
triphenylindium

: (E)-1-(2,6-dinitrophenyl)-2-phenyldiazene

: 99-65-0
meta-dinitrobenzene

: 92-52-4,1594-86-1
biphenyl

: 5110-81-6
2,6-dinitrobiphenyl

Guidance literature:: bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 20 ℃; for 0.0833333h;
DOI:10.1002/ejoc.200600527

Reference yield: 84.0%

: 5110-81-6
2,6-dinitrobiphenyl

: 84251-02-5
2-amino-6-nitro-1,1'-biphenyl

Guidance literature:: With ammonium sulfide; In pyridine; ethanol; for 3h; Heating;

Reference yield:

: 5110-81-6
2,6-dinitrobiphenyl

: 84251-59-2
2',2-diamino-4,6'-dimethoxy-m-quaterphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: hexamethylphosphoric acid triamide / 22 h

2: hydrazine hydrate / Pd/C / ethanol / 3 h / 80 °C

3: 49 mg / aq. HCl / ethanol / 2 h / Heating

With hydrogenchloride; hydrazine hydrate; palladium on activated charcoal; In N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol;