9H-Cyclopenta(b)quinolin-9-one, 1,2,3,4,5,6,7,8-octahydro-

Base Information

• Chemical Name: 9H-Cyclopenta(b)quinolin-9-one, 1,2,3,4,5,6,7,8-octahydro-
• CAS No.: 58596-34-2
• Molecular Formula: C12H15NO
• Molecular Weight: 189.2536
• DSSTox Substance ID: DTXSID40207314
• Wikidata: Q83081209

Synonyms:BRN 1528816;9H-Cyclopenta(b)quinolin-9-one, 1,2,3,4,5,6,7,8-octahydro-;58596-34-2;1,2,3,4,5,6,7,8-Octahydro-9H-cyclopenta(b)quinolin-9-one;5-21-08-00161 (Beilstein Handbook Reference);DTXSID40207314;LS-58218

Chemical Property of 9H-Cyclopenta(b)quinolin-9-one, 1,2,3,4,5,6,7,8-octahydro-

Chemical Property:

• Vapor Pressure: 2.95E-05mmHg at 25°C
• Boiling Point: 356.3°Cat760mmHg
• Flash Point: 154.1°C
• Density: 1.17g/cm³
• XLogP3: 2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 189.115364102
• Heavy Atom Count: 14
• Complexity: 363

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC2=C(C1)C(=O)C3=C(N2)CCC3

Technology Process of 9H-Cyclopenta(b)quinolin-9-one, 1,2,3,4,5,6,7,8-octahydro-

There total 1 articles about 9H-Cyclopenta(b)quinolin-9-one, 1,2,3,4,5,6,7,8-octahydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1,2,3,4,5,6,7,8-octahydro-cyclopenta[b]quinolin-9-one (58596-34-2)

Guidance literature:

Pyridin (Ie), Polyphosphorsaeure;

DOI:10.1007/BF00475956

Reference yield:

1,2,3,4,5,6,7,8-octahydro-cyclopenta[b]quinolin-9-one (58596-34-2) → 9-methylamino-2,3,5,6,7,8-hexahydro-1H-cycloheptaquinoline (125080-92-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / Et₃N*HCl, POCl₃ / 0.67 h / 60 °C

2: 97 percent / H₂O; ethanol / 18 h / 210 °C

With triethylamine hydrochloride; trichlorophosphate; In ethanol; water;

DOI:10.1007/BF00764431

Downstream raw materials:

9-methylamino-2,3,5,6,7,8-hexahydro-1H-cycloheptaquinoline

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