Technology Process of 1-Chloro-3-(pentyloxy)benzene
There total 1 articles about 1-Chloro-3-(pentyloxy)benzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: aluminum (III) chloride / dichloromethane / 2 h / 5 - 20 °C / Inert atmosphere
2: hydroxylamine hydrochloride / ethanol / 5 h / Reflux; Inert atmosphere
With
aluminum (III) chloride; hydroxylamine hydrochloride;
In
ethanol; dichloromethane;
1: |Friedel-Crafts Acylation;
DOI:10.1039/c3nj00032j
- Guidance literature:
-
Multi-step reaction with 6 steps
1: aluminum (III) chloride / dichloromethane / 2 h / 5 - 20 °C / Inert atmosphere
2: hydroxylamine hydrochloride / ethanol / 5 h / Reflux; Inert atmosphere
3: sodium tetrahydroborate; iodine / tetrahydrofuran / 7.5 h / 0 °C / Reflux; Inert atmosphere
4: triethylamine / tetrahydrofuran / 2 h / 5 - 20 °C / Inert atmosphere
5: thionyl chloride / toluene / 3 h / 80 °C / Inert atmosphere
6: sodium hydroxide / methanol / 1 h / 50 °C / Inert atmosphere
With
aluminum (III) chloride; sodium tetrahydroborate; thionyl chloride; hydroxylamine hydrochloride; iodine; triethylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; toluene;
1: |Friedel-Crafts Acylation;
DOI:10.1039/c3nj00032j
