Phosphoramidic dichloride, (4-bromophenyl)-

Base Information

• Chemical Name: Phosphoramidic dichloride, (4-bromophenyl)-
• CAS No.: 51250-38-5
• Molecular Formula: C6H5BrCl2NOP
• Molecular Weight: 288.89400
• Mol file: 51250-38-5.mol

Synonyms:N-4-bromophenylphosphoramidic dichloride;p-Bromanilin-N-oxychlorphosphin;

Chemical Property of Phosphoramidic dichloride, (4-bromophenyl)-

Chemical Property:

• PSA: 38.91000
• LogP: 4.51970

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phosphoramidic dichloride, (4-bromophenyl)-

There total 1 articles about Phosphoramidic dichloride, (4-bromophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromoaniline hydrochloride (624-19-1) → N-4-bromophenylphosphoramidic dichloride (51250-38-5)

Guidance literature:

With trichlorophosphate;

Reference yield: 73.0%

piperidine (110-89-4) + N-4-bromophenylphosphoramidic dichloride (51250-38-5) → N-4-bromophenyl-N',N''-bis(piperidinyl)phosphoric triamide

Guidance literature:

In acetonitrile; at -5 ℃; for 5h;

DOI:10.1016/j.poly.2010.09.039

Reference yield: 68.0%

N-4-bromophenylphosphoramidic dichloride (51250-38-5) + Trimethylenediamine (109-76-2,54018-94-9) → 2-(4-bromoanilino)-1,3,2-diazaphosphorinane-2-oxide

Guidance literature:

for 10h;

DOI:10.1246/bcsj.79.1604

upstream raw materials:

4-bromoaniline hydrochloride

Downstream raw materials:

(4-bromo-phenyl)-amidophosphoric acid diphenyl ester

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