Dibenzofuran-3-carbaldehyde

Base Information

Chemical Name:Dibenzofuran-3-carbaldehyde
CAS No.:51818-91-8
Molecular Formula:C13H8O2
Molecular Weight:196.20100
Hs Code.:2932999099
DSSTox Substance ID:DTXSID80541729
Nikkaji Number:J89.649G
Wikidata:Q82418164
Mol file:51818-91-8.mol

Synonyms:Dibenzofuran-3-carbaldehyde;51818-91-8;Dibenzo[b,d]furan-3-carbaldehyde;3-Dibenzofurancarbaldehyde;3-Dibenzofurancarboxaldehyde;SCHEMBL2533931;DTXSID80541729;KNGNDRNAPDAOJU-UHFFFAOYSA-N;AKOS006316744;AT33039;SB37466

Suppliers and Price of Dibenzofuran-3-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Dibenzofuran-3-carbaldehyde

Chemical Property:

Boiling Point:360.5±15.0 °C(Predicted)
PSA：30.21000
Density:1.289±0.06 g/cm3(Predicted)
LogP:3.39850
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:196.052429494
Heavy Atom Count:15
Complexity:251

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=C(O2)C=C(C=C3)C=O

Technology Process of Dibenzofuran-3-carbaldehyde

There total 6 articles about Dibenzofuran-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 4-iodo-3-phenoxybenzaldehyde

: 51818-91-8
dibenzofuran-3-carboxaldehyde

Guidance literature:: With palladium 10% on activated carbon; sodium acetate; In N,N-dimethyl acetamide; at 140 ℃; for 16h;
DOI:10.1021/acs.joc.5b00634

Reference yield:

: 26608-06-0
3-bromodibenzofuran

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 51818-91-8
dibenzofuran-3-carboxaldehyde

Guidance literature:: 3-bromodibenzofuran; With tert.-butyl lithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 0.166667h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -78 ℃;

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 51818-91-8
dibenzofuran-3-carboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: Trimethylacetic acid / 1,2-dichloro-ethane / 12 h / 80 °C

2: sodium acetate; palladium 10% on activated carbon / N,N-dimethyl acetamide / 16 h / 140 °C

With palladium 10% on activated carbon; sodium acetate; Trimethylacetic acid; In N,N-dimethyl acetamide; 1,2-dichloro-ethane;
DOI:10.1021/acs.joc.5b00634