1,6-Bis(triethoxysilyl)hexane

Base Information

• Chemical Name: 1,6-Bis(triethoxysilyl)hexane
• CAS No.: 52034-16-9
• Molecular Formula: C18H42O6Si2
• Molecular Weight: 410.699
• Mol file: 52034-16-9.mol

Synonyms:3,12-Dioxa-4,11-disilatetradecane,4,4,11,11-tetraethoxy;

Chemical Property of 1,6-Bis(triethoxysilyl)hexane

Chemical Property:

• Refractive Index: 1.42
• Boiling Point: 115 °C/0.05 mmHg
• PSA: 55.38000
• LogP: 4.64360

Purity/Quality:

99%, ^*data from raw suppliers

1,6-Bis(triethoxysilyl)hexane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,6-Bis(triethoxysilyl)hexane

There total 2 articles about 1,6-Bis(triethoxysilyl)hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

1,5-Hexadien (592-42-7) + Triethoxysilane (998-30-1) → 1,6-bis(triethoxysilyl)-n-hexane (52034-16-9)

Guidance literature:

dichlorobis(diethyl sulfide)platinum; In benzene; for 24h; Heating;

DOI:10.1016/0022-328X(86)82009-5

Reference yield:

→ 1,6-bis(triethoxysilyl)-n-hexane (52034-16-9)

Guidance literature:

entspr. Chlorsilan, Ethanol;

Reference yield: 81.2%

1,6-bis(triethoxysilyl)-n-hexane (52034-16-9) + 1,3,5,7,9,11,14-heptacyclopentyltricyclo[7.3.3.15,11]heptasiloxane-endo-3,7,14-triol (183387-28-2,135225-24-0) → C76H138O24Si16

Guidance literature:

With tetramethyl ammoniumhydroxide; In methanol; ethanol; at 0 - 5 ℃; for 24h; Cooling with ice;

DOI:10.1007/s10973-015-4655-4

upstream raw materials:

1,5-Hexadien

Triethoxysilane

Downstream raw materials:

Diethyl carbonate

Refernces

• 1、 Birkofer, Leonhard,Grafen, Klaus. "SILICIUMORGANISCHE VERBINDUNGEN LXXXVIII. DISILATRANYLALKANE". . p. 143 - 148. Retrieved 2007/10/02.