Technology Process of 2,6-Diaminoacridin-9(10H)-one
There total 22 articles about 2,6-Diaminoacridin-9(10H)-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium sulfide; sodium hydroxide;
In
ethanol; water;
at 20 ℃;
for 20h;
Heating / reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: iron; aqueous hydrochloric acid
2: aqueous sodium carbonate-solution
3: potassium carbonate; copper; amyl alcohol
4: H2SO4
With
hydrogenchloride; pentan-1-ol; sulfuric acid; iron; copper; sodium carbonate; potassium carbonate;
DOI:10.1039/jr9460000102
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; copper; copper(II) sulfate / water / 6 h / Reflux; Inert atmosphere
2: sulfuric acid / 1.75 h / 100 °C
3: sodiumsulfide nonahydrate; sodium hydroxide / water; ethanol / 28 h / Reflux
With
sodiumsulfide nonahydrate; sulfuric acid; copper; potassium carbonate; copper(II) sulfate; sodium hydroxide;
In
ethanol; water;
DOI:10.1021/jm5018303