5-ACETAMIDONAPHTHALENE-1-SULFONYL CHLORIDE

Base Information

• Chemical Name: 5-ACETAMIDONAPHTHALENE-1-SULFONYL CHLORIDE
• CAS No.: 52218-37-8
• Molecular Formula: C12H10ClNO3S
• Molecular Weight: 283.735
• Hs Code.: 2924299090
• European Community (EC) Number: 813-549-3
• DSSTox Substance ID: DTXSID80407492
• Wikidata: Q82212767
• Mol file: 52218-37-8.mol

Synonyms:5-(Acetylamino)naphthalene-1-sulfonyl chloride;

Chemical Property of 5-ACETAMIDONAPHTHALENE-1-SULFONYL CHLORIDE

Chemical Property:

• Appearance/Colour: Yellow solid
• Vapor Pressure: 1.5E-10mmHg at 25°C
• Melting Point: 188 °C dec
• Refractive Index: 1.655
• Boiling Point: 510.8 °C at 760 mmHg
• PKA: 13.18±0.43(Predicted)
• Flash Point: 262.7 °C
• PSA: 75.11000
• Density: 1.467 g/cm³
• LogP: 4.45600
• Storage Temp.: -20°C Freezer
• Solubility.: Acetonitrile (Slightly), Chloroform (Slightly, Heated)
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 283.0069920
• Heavy Atom Count: 18
• Complexity: 418

Purity/Quality:

97% ^*data from raw suppliers

5-Acetamidonaphthalene-1-sulfonylChloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)NC1=CC=CC2=C1C=CC=C2S(=O)(=O)Cl

Technology Process of 5-ACETAMIDONAPHTHALENE-1-SULFONYL CHLORIDE

There total 8 articles about 5-ACETAMIDONAPHTHALENE-1-SULFONYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C14H13NO5S → N-[5-(Chlorosulfonyl)-1-naphthalenyl]acetamide (52218-37-8)

Guidance literature:

With thionyl chloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h;

DOI:10.1016/j.dyepig.2015.09.031

Reference yield: 72.0%

sodium 5-acetamido-1-naphthalenesulfonate (102568-35-4) → N-[5-(Chlorosulfonyl)-1-naphthalenyl]acetamide (52218-37-8)

Guidance literature:

With chlorosulfonic acid; at 20 ℃;

Reference yield:

5-acetamidonaphthalene-1-sulfonic acid (691357-82-1) → N-[5-(Chlorosulfonyl)-1-naphthalenyl]acetamide (52218-37-8)

Guidance literature:

With phosphorus pentachloride;

DOI:10.1021/jm00029a001

upstream raw materials:

5-acetamidonaphthalene-1-sulfonic acid

sodium 5-acetamido-1-naphthalenesulfonate

1-aminonaphthalene-5-sulfonic acid

acetic anhydride

Downstream raw materials:

N-[5-[[(2-phenylethyl)amino)sulfonyl]-1-naphthalenyl]acetamide

N-[5-[(phenylamino)sulfonyl]-1-naphthalenyl]acetamide

N-(5-o-tolylsulfamoyl-naphthalen-1-yl)-acetamide

N-[5-(4-fluoro-phenylsulfamoyl)-naphthalen-1-yl]-acetamide

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