Benzenethiol, 4-methyl-, copper(1+) salt

Base Information Edit

Chemical Name:Benzenethiol, 4-methyl-, copper(1+) salt
CAS No.:52403-06-2
Molecular Formula:C7H8S.Cu
Molecular Weight:186.745
Hs Code.:
Mol file:52403-06-2.mol

Synonyms:

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Chemical Property of Benzenethiol, 4-methyl-, copper(1+) salt Edit

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Technology Process of Benzenethiol, 4-methyl-, copper(1+) salt

There total 13 articles about Benzenethiol, 4-methyl-, copper(1+) salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1292766-17-6
copper(I) thiophene-2-carboxylate

: 6783-05-7
trans-2-phenylvinylboronic acid

: 75072-07-0
S-(trifluoroacetyl)-p-methylthiophenol

: B(OH)2(C₄H₃SCOO)

: 3108-32-5,86571-25-7
(E)-1,1,1-trifluoro-4-phenyl-3-buten-2-one

: 52403-06-2
p-tolylthiolatocopper(I)

Guidance literature:: With Pd₂(dba)3*CHCl₃/tris(2-furyl)phosphine; In tetrahydrofuran; addn. of 1.6 equiv. of C4H3SCOOCu to the reaction of CF3COSC6H4CH3 (1 equiv.) with (CHCHC6H5)B(OH)2 (1 equiv.) in THF in presence of 1% Pd2(dba)3*CHCl3/(tris-2-furylphosphine), holding for 18 h at 50°C;
DOI:10.1021/ja005613q

Reference yield: 88.0%

: 1292766-17-6
copper(I) thiophene-2-carboxylate

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 318257-80-6
2-acetoxythioacetic acid S-p-tolyl ester

: B(OH)2(C₄H₃SCOO)

: 52403-06-2
p-tolylthiolatocopper(I)

: 4-(2-acetoxyacetyl)benzoic acid methyl ester

Guidance literature:: With Pd₂(dba)3*CHCl₃/tris(2-furyl)phosphine; In tetrahydrofuran; addn. of 1.6 equiv. of C4H3SCOOCu to the reaction of CH3COOCH2COSC6H4CH3 (1 equiv.) with (CH3OOCC6H4)B(OH)2 (1 equiv.) in THF in presence of 1%Pd2(dba)3*CHCl3/(tris-2-furylphosphine), holding for 18 h at 50°C;
DOI:10.1021/ja005613q