Benzene, 1-chloro-2-isothiocyanato-4-methyl-

Base Information

• Chemical Name: Benzene, 1-chloro-2-isothiocyanato-4-methyl-
• CAS No.: 52747-70-3
• Molecular Formula: C₈H₆ClNS
• Molecular Weight: 183.661
• Mol file: 52747-70-3.mol

Synonyms:Benzene,1-chloro-2-isothiocyanato-4-methyl;2-Chloro-5-methylphenylisothiocyanate;

Chemical Property of Benzene, 1-chloro-2-isothiocyanato-4-methyl-

Chemical Property:

• PSA: 44.45000
• LogP: 3.38270

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzene, 1-chloro-2-isothiocyanato-4-methyl-

There total 2 articles about Benzene, 1-chloro-2-isothiocyanato-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiophosgene (463-71-8) + 2-chloro-5-methylaniline (95-81-8) → 1-chloro-2-isothiocyanato-4-methyl-benzene (52747-70-3)

Guidance literature:

With chloroform; water;

DOI:10.1039/jr9310003285

Reference yield:

→ 1-chloro-2-isothiocyanato-4-methyl-benzene (52747-70-3)

Guidance literature:

Reference yield: 65.0%

1-chloro-2-isothiocyanato-4-methyl-benzene (52747-70-3) + 2-hydrazinocarbonyl-3,5-dichlorobenzo[b]thiophene (628724-62-9) → C17H12Cl3N3OS2

Guidance literature:

In ethanol; Heating;

upstream raw materials:

thiophosgene

2-chloro-5-methylaniline

Downstream raw materials:

5-(2-chloro-5-methyl-anilino)-[1,2,4]thiadiazol-3-one