[(4-Chlorophenyl)(phenyl)methylidene]hydrazine

Base Information

• Chemical Name: [(4-Chlorophenyl)(phenyl)methylidene]hydrazine
• CAS No.: 55816-27-8
• Molecular Formula: C13H11ClN2
• Molecular Weight: 230.697
• European Community (EC) Number: 665-382-9
• DSSTox Substance ID: DTXSID30971219
• Mol file: 55816-27-8.mol

Synonyms:55816-27-8;[(4-chlorophenyl)(phenyl)methylidene]hydrazine;DTXSID30971219

Chemical Property of [(4-Chlorophenyl)(phenyl)methylidene]hydrazine

Chemical Property:

• Vapor Pressure: 3.49E-05mmHg at 25°C
• Boiling Point: 353.8°Cat760mmHg
• Flash Point: 167.8°C
• Density: 1.17g/cm³
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 230.0610761
• Heavy Atom Count: 16
• Complexity: 238

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=NN)C2=CC=C(C=C2)Cl

Technology Process of [(4-Chlorophenyl)(phenyl)methylidene]hydrazine

There total 1 articles about [(4-Chlorophenyl)(phenyl)methylidene]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-chlorobenzophenone (134-85-0) → 4-chlorobenzophenone hydrazone (55816-27-8)

Guidance literature:

With hydrazine hydrate; In water; butan-1-ol; Reflux;

DOI:10.1007/s12272-012-0608-7

Reference yield: 86.0%

4-chlorobenzophenone hydrazone (55816-27-8) → 1-chloro-4-(diazo(phenyl)methyl)benzene (1140-33-6)

Guidance literature:

1-methylimidazole ligand; In acetonitrile; for 0.333333h;

DOI:10.1246/cl.1986.505

Reference yield: 86.0%

4-chlorobenzophenone hydrazone (55816-27-8) → 4-chlorobenzophenone azine

Guidance literature:

With copper acetylacetonate; oxygen; Heating;

upstream raw materials:

4-chlorobenzophenone

Downstream raw materials:

4-chlorophenyl(phenyl)methane

1-chloro-4-(diazo(phenyl)methyl)benzene

bis-(4-chloro-benzhydrylidene)-hydrazine

4-chlorobenzophenone (diphenylacetyl)hydrazone